shroombee, here is my list of potential small improvements/modifications/updates to the current published tek (
69ron's lime/limo starting with 1:3:0.25 cactus powder:water:lime)
1) Make the initial paste more workable by
microwaving in short bursts (make sure it does not overflow the jar when boiling) and stirring to half the initial weight of water (use a food scale to keep track), add 20% of remaining water weight as salt and mix well. This process is will cause some ammonia smell.
2) During the Limonene pulls, warm the jar in a water bath. Mix slowly but well (don't whip it up into a Limonene souffle) and allow resting time for Limonene to sweat out of the paste. You should be able to easily pour off the Limonene.
3) After pulling, let the Limonene rest until it is crystal clear and no new sediment forms (e.g. tiny water drops). Decant off the settled Limonene.
4) Use sulfuric acid drops (e.g. 10% used for aquariums) for water salting and monitor pH shooting for ~6.5. A separatory funnel or color indicator makes this easier. Lower pH could pull lower pKa stuff making the extraction less clean. Since salt is insoluble in Limonene (unlike FB which is soluble in both water and Limonene), one salting is enough, just make sure pH is stable at ~6.5 after further shaking. Skip your arm workout day.
6) Reuse the salted Limonene on a new pull and monitor how many sulfuric drops are needed to salt it to pH 6.5. Keep pulling as long as mescaline FB is coming through (one 25ml 10% sulfuric drop neutralizes about 10mg of FB mescaline, so counting drops at helps know when to stop). The drops should follow a
geometric series (ratio of drops between pulls constant, for example 100, 60, 36, 22, 13, 8, 5).
7) Combine saltings and precipitate using
dg's water reduction and acetone xtalization. Add acetone slowly and stop when cloudy. Adding excess acetone could precipitate other stuff.
8 ) Optionally clean up further with more re-Xs
9) The biggest shiniest xtals I've seen appear after dissolving in water and letting that slowly evaporate over time.
I'm sure I'm missing stuff. Also, some of this could be wrong. The microwaved paste is stinky (likely ammonia from plant stuff breaking down) and is hot/caustic, I have used mason jars without issues, but each person should make their own decision after understanding the process. To the best of my knowledge it works well for me based on trial and error. Cheers.