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Jar broke in heat bath Options
 
Dirt
#1 Posted : 3/29/2020 8:08:47 PM

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Quick question, there was a mason jar that was being warmed up in a water bath that the bottom broke out of.Shocked The contents were post defat ACRB, already added SH to ph ~13 and was warming to start pulls. Contents mixed with the bath water cleanly, but is now obviously much more diluted.
1. Can it be reduced by boiling down or will the contents also evap?
2. If it can be reduced, will the steam be dangerous due to the content of SH?
3. Or should the new, diluted solution be brought to correct ph and do more pulls and let plenty more naph evap before freeze precipitation?


Thanks
 

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Eaglepath
#2 Posted : 3/29/2020 8:40:25 PM

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Hahaha this happend to me so many times.. its amazing every time..Smile

Just put all the liquid in different jars and check so the PH is good then pull as usual.

And be happy that you had a heat bath and not just a sink haha
"Too cute to live, too cozy to die" - Eaglepath
 
Dirt
#3 Posted : 3/29/2020 9:47:07 PM

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Thanks EaglepathThumbs up
 
downwardsfromzero
#4 Posted : 3/30/2020 12:54:14 AM

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It's great when the heat bath saves your brew, eh? Happened to me too.




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Dirt
#5 Posted : 3/30/2020 3:39:20 AM

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After 6 hours of brew time..... yes indeed!
 
La Alquimista
#6 Posted : 4/3/2020 9:35:32 PM
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If pH is increased to pull as was done in OP it will be fine, but to make sure that the solvent is shaken well through the large volume and allowed to settle several times. Keep solution until yield is recorded, if it is lower than past yields more extractions may be required.
 
Dirt
#7 Posted : 4/9/2020 1:04:17 AM

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La Alquimista wrote:
If pH is increased to pull as was done in OP it will be fine, but to make sure that the solvent is shaken well through the large volume and allowed to settle several times. Keep solution until yield is recorded, if it is lower than past yields more extractions may be required.



Thanks La Alquimista, All went well, just had A lot of Pre-evaperating of Napth due to the new increased volume.
 
 
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