CHATPRIVACYDONATELOGINREGISTER
DMT-Nexus
FAQWIKIHEALTH & SAFETYARTATTITUDEACTIVE TOPICS
«PREV456
Mimosa hostilis and extract analysis thread (FASA, FASW, Naphtha, Limo, "jungle spice" etc Options
 
pitubo
#101 Posted : 12/28/2017 9:33:13 PM

dysfunctional word machine

Senior Member

Posts: 1831
Joined: 15-Mar-2014
Last visit: 11-Jun-2018
Location: at the center of my universe
Brennendes Wasser,

Thank you for performing this analysis! This is valuable data that has not been posted before at the nexus. Congratulations with your promotion.

I don't understand why you got such a snarky response initially. Though I agree with the remark that a mention of the species of the plant from which the tested extract was made would have been in order and some details about the analytical gear would have been nice. After all, science is about reproducibility.

For the rest, I think that the graphs are pretty clear and not messy at all. Furthermore, we do have some nexus members who are very knowledgeable in matters of chemical analysis in general and nmr spectroscopy in particular. I can't see why this information should not be presented or discussed in depth here.

IMHO the information that you posted belongs in the RESEARCH section, probably in the "Plant Analysis and Substance Testing" subforum. In fact, I think that it would be a good addition to the thread that endlessness pointed to.
 

Trippy glass for trippy people.
 
downwardsfromzero
#102 Posted : 1/4/2018 12:01:34 AM

Comical egg spurt; Senile mumbler

Chemical expertSenior Member

Posts: 4358
Joined: 30-Aug-2008
Last visit: 14-Dec-2019
Location: square root of minus one
Brennendes Wasser,

Is there any chance you could supplement this data by the addition of the spectra for 2-methyltetrahydrobetacarboline? I get the feeling this might be rather useful.
Ora, lege, lege, lege, relege et labora

“To be GOVERNED is to be watched, inspected, spied upon, directed, law-driven, numbered, regulated, enrolled, indoctrinated, preached at, controlled, checked, estimated, valued, censured, commanded, by creatures who have neither the right nor the wisdom nor the virtue to do so. To be GOVERNED is to be at every operation, at every transaction noted, registered, counted, taxed, stamped, measured, numbered, assessed, licensed, authorized, admonished, prevented, forbidden, reformed, corrected, punished. It is, under pretext of public utility, and in the name of the general interest, to be place under contribution, drilled, fleeced, exploited, monopolized, extorted from, squeezed, hoaxed, robbed; then, at the slightest resistance, the first word of complaint, to be repressed, fined, vilified, harassed, hunted down, abused, clubbed, disarmed, bound, choked, imprisoned, judged, condemned, shot, deported, sacrificed, sold, betrayed; and to crown all, mocked, ridiculed, derided, outraged, dishonored. That is government; that is its justice; that is its morality."
― Pierre-Joseph Proudhon
 
Brennendes Wasser
#103 Posted : 7/15/2018 5:22:59 PM

DMT-Nexus member


Posts: 331
Joined: 23-Sep-2017
Last visit: 21-Sep-2019
Sorry for long time no look into this!

Well I was about to take a spectra of my Harmaline / Harmine mixture, which would be interesting of course by its own, but also to identify how pure it is by the method I did (and nearly all of us do) AND to identify what is the ratio between Harmaline and Harmine.

Sadly the Freebase does not dissolve in MeOD, not in DMSO, not in CDCl3.

Of course to a lesser extent so that the solvent gets coloured, but just by eye I would say that 90%+ stays undissolved ...

Therefore with that Freebase I had no chance to get a suitable sample for a NMR Analysis. I also tried the Salt Form, but 20 mg did also not dissolve in 0,6 ml Water, only to a negligible extent. Even heating the solvents to their vap temp did not change anything. Therefore I have abandoned this so far, but possibly I may try it later.



But beware, I have other good news!!

I have more analysis to share with you and this time much more interesting and also much more data.

I just would prefer to start an own thread ... because of 2 Reasons.

A) I will possibly expand that post over time more and more and it would be nice if every info is as compressed as possible.

B) If I post it here is may somehow get *lost* and overseen as this thread may expand further in the future.


Therefore it would be cool if I would be allowed to start a new thread, which won't get merged into this one.
Check the

BIG Analysis on DMT !

Lots of interesting and possibly new stuff unraveled ;o
 
Brennendes Wasser
#104 Posted : 7/26/2018 1:50:51 PM

DMT-Nexus member


Posts: 331
Joined: 23-Sep-2017
Last visit: 21-Sep-2019
Ok here it is:

My THREAD FOR BIG DMT ANALYSIS !


THXXX !!!!
Check the

BIG Analysis on DMT !

Lots of interesting and possibly new stuff unraveled ;o
 
«PREV456
 
Users browsing this forum
Guest

DMT-Nexus theme created by The Traveler
This page was generated in 0.028 seconds.