CHATPRIVACYDONATELOGINREGISTER
DMT-Nexus
FAQWIKIHEALTH & SAFETYARTATTITUDEACTIVE TOPICS
12NEXT
is 12.65 ph high enough for stb? Options
 
travinski
#1 Posted : 10/27/2008 2:21:12 AM

DMT-Nexus member


Posts: 160
Joined: 07-Oct-2008
Last visit: 05-Nov-2011
Location: kelowna
i used nomans stb and got a ph of 12.65 i did 180 grams mhrb and ive only got 3/4g back after recrystal and several pulls....8-9 also evapped my solvent and recrystalled that too but im thinkin i could or should be getting more back. any ideas anyone? also my bark has been sitting for a week str8 in the solution
travinski is an alter ego and not a real person, i also like to play dress up when im not playing fictional chemist
 

STS is a community for people interested in growing, preserving and researching botanical species, particularly those with remarkable therapeutic and/or psychoactive properties.
 
kemist
#2 Posted : 10/28/2008 10:54:11 AM

John


Posts: 700
Joined: 31-Aug-2008
Last visit: 22-May-2018
Location: Highland
With what solvent ?
As a kemist I never met ILPT in physical form and never talk to him. He share his wisdom, trough my mind, telepathicly only. Please don`t prosecute me, for his possible illegal activities. He is bonkers about chemistry and doesn`t even exist in this primitive reality !!!
 
travinski
#3 Posted : 10/28/2008 10:53:14 PM

DMT-Nexus member


Posts: 160
Joined: 07-Oct-2008
Last visit: 05-Nov-2011
Location: kelowna
lye, naptha pulls , bestine recrystal
travinski is an alter ego and not a real person, i also like to play dress up when im not playing fictional chemist
 
endlessness
#4 Posted : 10/29/2008 12:01:00 AM

DMT-Nexus member

Moderator

Posts: 12956
Joined: 19-Feb-2008
Last visit: 25-Jun-2018
Location: Jungle
3, 4 grams of spice out of 180g of MHRB and you think its too little?!

man, basically nobody gets a 2% yield, most people get half or even a quarter of that! be happy!
 
travinski
#5 Posted : 10/29/2008 2:20:26 AM

DMT-Nexus member


Posts: 160
Joined: 07-Oct-2008
Last visit: 05-Nov-2011
Location: kelowna
no no no dude i would be stoked if i had that i got 3 quarters of a gram (3/4)
travinski is an alter ego and not a real person, i also like to play dress up when im not playing fictional chemist
 
Jorkest
#6 Posted : 10/29/2008 2:35:06 AM

DMT-Nexus member

Moderator | Skills: Extraction Troubleshooting, (S)elf ProgrammingChemical expert | Skills: Extraction Troubleshooting, (S)elf Programming

Posts: 4338
Joined: 02-Oct-2008
Last visit: 10-May-2018
how much lye did you use?

and did you heat up the solvent and lye/mimosa mix while you pulled? 130degreesF is as hot as you want to go...but heating is very important
it's a sound
 
travinski
#7 Posted : 10/29/2008 2:38:02 AM

DMT-Nexus member


Posts: 160
Joined: 07-Oct-2008
Last visit: 05-Nov-2011
Location: kelowna
followed nomans tek 1g per g of bark
travinski is an alter ego and not a real person, i also like to play dress up when im not playing fictional chemist
 
travinski
#8 Posted : 10/29/2008 2:42:52 AM

DMT-Nexus member


Posts: 160
Joined: 07-Oct-2008
Last visit: 05-Nov-2011
Location: kelowna
nope no heat can i do that i have a 4 litre jug of this crap ill have to check if i have something big enough and do i heat the whole time while separating?
....im thinking hot water bath?
travinski is an alter ego and not a real person, i also like to play dress up when im not playing fictional chemist
 
endlessness
#9 Posted : 10/29/2008 2:46:38 AM

DMT-Nexus member

Moderator

Posts: 12956
Joined: 19-Feb-2008
Last visit: 25-Jun-2018
Location: Jungle
.75 for 180g is not so good but its not horribly bad either

was the bark finely powdered? if not, that could be one of the reasons..

the last pulls should be with hot solvent. (hot water bath on some solvent and then throw it in.. or one can even do a hot water bath on the whole jug but I dont think its necessary)


and maybe the bark was not so good to begin with.. ?
 
travinski
#10 Posted : 10/29/2008 2:50:49 AM

DMT-Nexus member


Posts: 160
Joined: 07-Oct-2008
Last visit: 05-Nov-2011
Location: kelowna
well i did a small test batch with 50 g and got back .5 of white crystals when i did the 180g i did the exact same thing as before but with way different results. the last pulls with hot solvent doesnt make sense to me though coz when you put hot solvent in, it cools in the bark mix.... leaving you with once again cool solvent any extra dmt the hot solvent would carry you would think should drop out when the solvent cools
travinski is an alter ego and not a real person, i also like to play dress up when im not playing fictional chemist
 
Jorkest
#11 Posted : 10/29/2008 3:01:13 AM

DMT-Nexus member

Moderator | Skills: Extraction Troubleshooting, (S)elf ProgrammingChemical expert | Skills: Extraction Troubleshooting, (S)elf Programming

Posts: 4338
Joined: 02-Oct-2008
Last visit: 10-May-2018
just do a hot water bath...it will help a lot...
it's a sound
 
travinski
#12 Posted : 10/29/2008 3:24:53 AM

DMT-Nexus member


Posts: 160
Joined: 07-Oct-2008
Last visit: 05-Nov-2011
Location: kelowna
does it matter how long the barks been sitting in the basified solution its been about 2 -3 weeks
travinski is an alter ego and not a real person, i also like to play dress up when im not playing fictional chemist
 
Jorkest
#13 Posted : 10/29/2008 3:28:56 AM

DMT-Nexus member

Moderator | Skills: Extraction Troubleshooting, (S)elf ProgrammingChemical expert | Skills: Extraction Troubleshooting, (S)elf Programming

Posts: 4338
Joined: 02-Oct-2008
Last visit: 10-May-2018
no that shouldnt do anything...SWIM has had stuff sitting for months AFTER doing the extraction but left the solvent on top...and then decided to get it cleaned up..so he poured off the solvent and was able to get a nice chunk(1.5g) from it...nice crystals...slightly yellow..but he hasnt rextalized yet
it's a sound
 
travinski
#14 Posted : 10/29/2008 3:47:09 AM

DMT-Nexus member


Posts: 160
Joined: 07-Oct-2008
Last visit: 05-Nov-2011
Location: kelowna
the bark has reached 115 f....and warming thanks dude ill let ya know what happens
travinski is an alter ego and not a real person, i also like to play dress up when im not playing fictional chemist
 
Jorkest
#15 Posted : 10/29/2008 3:59:47 AM

DMT-Nexus member

Moderator | Skills: Extraction Troubleshooting, (S)elf ProgrammingChemical expert | Skills: Extraction Troubleshooting, (S)elf Programming

Posts: 4338
Joined: 02-Oct-2008
Last visit: 10-May-2018
sweet dude
it's a sound
 
Noman
#16 Posted : 10/29/2008 4:41:20 AM

DMT-Nexus member

Senior Member

Posts: 1052
Joined: 18-Jan-2008
Last visit: 15-Jun-2018
Did your friend recover as much solvent as he put in?
Sometimes STB teks require extra water - 50 to 100 percent more - for the bark/caustic/naptha mix to separate fully.
 
kemist
#17 Posted : 10/29/2008 10:53:07 AM

John


Posts: 700
Joined: 31-Aug-2008
Last visit: 22-May-2018
Location: Highland
Sorry lads but this tek performed just with naphta is rubbish.The spice from naphta is very plain. ILPT did STB with leftover bark from A/B with DCM. MASSIVE PAIN IN THE ARSE, pals. you got emulsions to filter of and undissolved part of bark like to suck your dcm spice. But very powerful spice was recovered, after all this arsing. Jungle compound adding the lovely loop-iness to the DMT enlightenment it`s shame to avoid extraction of jungle. Toluene or other on water floating solvent(lovely Et2O )would definitely become more handy And you can start pull easily from ph 10-11 Laughing
As a kemist I never met ILPT in physical form and never talk to him. He share his wisdom, trough my mind, telepathicly only. Please don`t prosecute me, for his possible illegal activities. He is bonkers about chemistry and doesn`t even exist in this primitive reality !!!
 
travinski
#18 Posted : 10/29/2008 1:15:03 PM

DMT-Nexus member


Posts: 160
Joined: 07-Oct-2008
Last visit: 05-Nov-2011
Location: kelowna
i freeze precipped overnight the naptha went milky colored after the first hour but this morning theres notta, dang this sucks donkey balls...... oh well will keep trying
travinski is an alter ego and not a real person, i also like to play dress up when im not playing fictional chemist
 
acolon_5
#19 Posted : 10/29/2008 3:27:11 PM

The Great Namah


Posts: 3433
Joined: 18-Jan-2008
Last visit: 30-Nov-2014
Location: The place entites go when they smoke allspice
If you are using massive amounts of naphtha you will need to evap some of it. I usually only freeze precip when i have 100-200mL naphtha.

I never really liked the STB's too much waste (lye, naphtha)
The Spice extends life
The Spice expands consciousness
The Spice is vital for space travel
___________________________________________________________________________________________________
Never underestimate the power of STUFF!


I am certifiably insane, as such all posts written by me should be regarded as utter nonsense or attempts to get attention.

I don't know SWIM and personally don't trust him at all. If SWIM is posting, most likely I will not respond...as I said, I don't trust the guy. YOU I trust, but never SWIM.
 
travinski
#20 Posted : 10/29/2008 10:56:13 PM

DMT-Nexus member


Posts: 160
Joined: 07-Oct-2008
Last visit: 05-Nov-2011
Location: kelowna
ya this is my first extract and nomans seemed to be the easiest to follow, and quickest. i didnt want to do an a/b coz all the teks i read involved weeks to make it. but i guess it doesnt matter coz im into my 2nd or 3rd week messin with this 228 g's of bark with stb
travinski is an alter ego and not a real person, i also like to play dress up when im not playing fictional chemist
 
12NEXT
 
Users browsing this forum
Guest

DMT-Nexus theme created by The Traveler
This page was generated in 0.029 seconds.