This is the best that my friend has tried.
"You want to start with water. If you start with alcohol, it pulls out a TON of fat and oil from the beans. If you don't mind de-fatting your extract, alcohol will do fine. De-fatting is a drag. However always make sure to add calcium hydroxide at some point near the end of your extraction or you’ll end up with an acidic form of bufotenin which will make you sick.
Here’s a simple tech that anyone can do.
* Go to a country were this is 100% LEGAL! Do NOT do this in a country were it is not 100% legal to do so. Its legal in most countries. I like Brazil. Its not legal in the US. What's wrong with Americans? I thought this was the land of the free like the song says.
* Boil the powdered beans covered in plenty of water (made pH 3 with hydrochloric acid, or just use 1 part vinegar to 3 parts water). Filter out the beans. You might want to do this a few times to get all the alkaloids.
* Evaporate the water extract down to a syrupy consistency. You can use an oven at 175 F to evaporate your stuff if you like. It’s best to use a commercial food dehydrator for this.
* To your syrup add alcohol (91% isopropyl alcohol is great), enough to make it easy to poor. Mix it for a minute or so. Solids will forms.
* Filter out the solids that form and discard them.
* Evaporate your alcohol down to a syrupy consistency.
* To your thick syrup add calcium hydroxide (pickling lime for cooking), enough to make a paste. Mix it thoroughly. It should start to smell like ammonia. Let it sit for many hours. Once the ammonia smell is gone, the reaction is complete. Instead of aweful acidic bufotenine you now have the superior calcium bufotenate in your extract.
At this point you have two options:
Alcohol option:
* mix in a generous amount of alcohol to soak up the bufotenine. Filter out the solids, evaporate your alcohol to get a pretty good extract (about 30% calcium bufotenate). Break it up into a fine powder. About 5 mg is a good starting dose for vaporizing it.
Acetone option:
* dry your extract completely. Then break it up into a fine powder.
* mix in a generous amount of acetone (available as a 100% pure solvent at most hardware stores) to soak up the bufotenine. Filter out the solids, evaporate your acetone to get a pretty good extract (about 75% calcium bufotenate).
* dissolve your extract in just enough 91% isopropyl alcohol to make a thick syrup.
* add 2 parts water. Filter out and SAVE the solids. The solids are your calcium bufotenate and the water should be discarded. Now you have nearly 90% pure calcium bufotenate. About 2 mg is a good starting dose for vaporizing it. A 10 mg dose is VERY INTENSE. Note that a small amount of calcium bufotenate will be left in the water used. This can be saved and re-extracted later.
Either way, the final extract tends to be a little bit sticky, more so if you go the alcohol route. I recommend adding a little cellulose like pharmaceutical companies use. About 10-20% by weight is good. You can buy cellulose at health food stores. It’s sold as dietary fiber. Just weigh out your extract to calculate 10-20% of that weight in cellulose, add some alcohol to it, just enough to make a syrup, then mix your cellulose and let it dry again. It shouldn't be sticky anymore."
someone is trying this method now would of tried 69ron's but dont now how to get citric acid hope his extract is successfull i heard he love the visuals