Brennendes Wasser wrote:I have read briefly through your TEK but I still want to clarify this 1 question:
So with *1 single Pull* you mean 1 acidic cook instead of multiple?
And this 1 cook will give you up to 1,4 %?
As I maybe wrote that I also want to try 1 long instead of 2 short I wanna ask if you think that a lower time would also suffice?
In Max ION it is told to do 1 for 8 h and NOT stirr it. So do you use 12-24h because of the process to release that Tannins takes longer time and would instantly using HCl -> pH 3 make 8 hours be long enough or even less?
THXX ;D
I don't even really do a "cook." It's more like: Add the powdered material into a beaker or jar; add water until the total volume (including bark displacement) is roughly 500 mL; and let it stir with occasional heat. I didn't mind the longer duration because I rarely use DMT (anymore; I had my time.

). It was more of an experiment to see if the tannis could naturally acidify; and how much NaOH was actually needed to maintain a steady pH within the range I wanted.
The bark and the water are never separated from each other. The mix spins for "x" amount of time, with occasional heat (I never brought to a boil), and once the desired pH is achieved from the tannins, then it's ready to add the base.
So, for you, it wouldn't change much - if you have large pieces, then the method I proposed may not be worth your time. When I have used large pieces of bark, in the past, I did 3x 2 hr acid simmers and straining. Collecting all the separate portions and then reducing to a smaller volume of roughly 500 mL.
Unfortunately, Larger chunks can be more of a pain to get maximum yields.
When I mean a single pull, I am referring to the naphtha or heptane. Since the starting water never leaves the powdered bark, I guess you could call it a "cook," but the plant matter is never removed. It just sits there and the cells become lysed. Then add the amount of base that you need to get the bark/water/base mix to a pH of ~13. Then I use 250 - 300 mL of naphtha or heptane to do a single pull from the alkaline mix.
Take Care,
ACY
Sometimes it's good for a change. Other times it isn't.