I know this is very late but swim has recently found a way of reversing the brown naphtha. If the naphtha appears brown or reddish, remove from the heat and let the entire soup cool down to room temperature whilst rolling and tipping your vessel, (hourly).
SWIM let the soup stand at room temperature overnight and came back the next day and it was as though all the oils and unwanted impurities had fell back into the aqueous layer. Just to make sure Swim didn't lose any of the DMT, Swim then re-heated the soup at a lower temperature for 6 hours with rolling and tipping of the vessel hourly, as before, then proceeded with the pull.
swim knows you end up using another day and a half but it is definitely worth it. Swim usually yields very pale yellow or white spice normally, when darker yellow product is precipitated swim gets excited because swim knows the extra alkaloids are dam right tasty.
Also a very simple Re-crystalization method:
Put DMT crystals into a small beaker.
get a bowl full of warm water.
Put clean naphtha, about 75ml in with your crystals in the beaker.
Swirl your beaker with DMT and naphtha in the bowl of hot water till All DMT is dissolved.
(dark orange, brown or even red debris may appear at the bottom of the glass, do not worry if thas hasn't dissolved.
Place in freezer for 1 hour and you will see a dirty layer of oil at the bottom of the glass.
Syphon off the remaining DMT saturated Naptha then Freeze precipitate as normal.
This step can be repeated to field a purer product every time.
A few quick tips from SWIM:
When performing an STB extraction, when you have pulled your layer of saturated naphtha, Allow roughly 35-40% evaporation at room temperature. You will see the naphtha become a much more concentrated yellow as the excess naphtha has left.
Cover the Naptha solution and let sit at room temperature for a couple of hours, then proceed to place in the fridge for a few hours, then finally put in the freezer overnight. This was how SWIM first started fielding larger, more snow globe like crystals.
"Time is nothing but an artificial measurement"