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Results of SWIMs first extraction... Options
 
WhereEaglesDare
#1 Posted : 2/9/2014 5:26:57 PM
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So SWIM attempted his first extraction yesterday using Cyb's Hybrid ATB Salt Tek with 50 g MHRB. SWIM followed the instructions to the letter apart from having to us a smaller bottle (750 ml instead of a litre) so adjusted the amount de-ionised water added at the end to top up. Also SWIM only had 2 glass dishes available due to space in the freezer so SWIM put the final pull in a glass jug and evaporated some nps before freeze precipitation.

Here are SWIMs results..

(excuse the bad pics!):








First Glass dish yielded 0.680 mg as seen above.

Phoned battery died so SWIM hasn't got pics of the second dish/weight but it yielded lower, a lot less crystals, more wax/goo 0.300 mg.

Total yield from 2 dishes was 0.980 mg so almost a 2% yield and SWIM still have the jug in the freezer but it looks mainly like oil/goo which SWIM will re-x and free precip.

Swim has a couple of questions:

1) Currently SWIM has it stored in tin foil wraps (crystals in one, wax in one, powder in another) which are in a few plastic weed bags sealed in a larger air tight container in the freezer. Does DMT react with tin foil or plastic baggies?

2) The crystals look pure already so SWIM is not sure whether to re-x these but probably will. On average how much weight do you tend to lose from a re-x?

All in all a really enjoyable process and Cyb's tek is so easy for a noob to follow. SWIM can't wait to do the next one!


 

Good quality Syrian rue (Peganum harmala) for an incredible price!
 
cyb
#2 Posted : 2/9/2014 6:01:21 PM

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Well done. Wink

1. Please stop Swimming
2. Little vials are airtight and perfect for storing
3. No need for a Re-x...just try 15mg and work your way up 5mg at a time.

*End Transmission*
Please do not PM tek related questions
Reserve the right to change your mind at any given moment.
 
WhereEaglesDare
#3 Posted : 2/9/2014 6:30:07 PM
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Thanks Cyb.

So I shouldn't re-x the wax and goo to try and get it crystalline.

I will get some vials. Will tin foil react with dmt in the short term?
 
a1pha
#4 Posted : 2/9/2014 7:03:17 PM


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cyb wrote:
2. Little vials are airtight and perfect for storing

I haven't posted this link in awhile and now seems a good time: Specialty Bottle

Excellent selection and prices.

Enjoy that fluffy yumminess!
"Facts do not cease to exist because they are ignored." -A.Huxley
 
Earthwalker
#5 Posted : 2/9/2014 7:12:44 PM

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Good result !!

See all that worry for nothing , top stuff !!Thumbs up
 
arcologist
#6 Posted : 2/9/2014 7:18:07 PM

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a1pha wrote:
cyb wrote:
2. Little vials are airtight and perfect for storing

I haven't posted this link in awhile and now seems a good time: Specialty Bottle


I second this place, great source for all storage needs. I like the JAM1 on this page because it has a larger opening than the vials but isn't too big either. The one downside is that I usually pay more for shipping than the glassware itself.
 
Earthwalker
#7 Posted : 2/9/2014 7:30:41 PM

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I just bought some 5 ml bottles I just hope there not to small ,, but I did but 10 !!
 
WhereEaglesDare
#8 Posted : 2/9/2014 7:32:05 PM
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Thanks everyone, I am in UK so looking for vials. Just worried foil might react in the short term. I though about making paper wraps (like cocaine) and putting in those then in baggies in an airtight jar.

 
Earthwalker
#9 Posted : 2/9/2014 7:42:35 PM

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WhereEaglesDare wrote:
Thanks everyone, I am in UK so looking for vials. Just worried foil might react in the short term. I though about making paper wraps (like cocaine) and putting in those then in baggies in an airtight jar.


Careful I wrapped some in a cigaret paper once only to have it melt or soak into the paper , so be careful and make sure you're paper isn't absorbent in any way !!
 
3rdI
#10 Posted : 2/9/2014 7:44:29 PM

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WhereEaglesDare wrote:
Thanks everyone, I am in UK so looking for vials. Just worried foil might react in the short term. I though about making paper wraps (like cocaine) and putting in those then in baggies in an airtight jar.


a vial for changa and one for crystals
INHALE, SURVIVE, ADAPT

it's all in your mind, but what's your mind???

fool of the year

 
WhereEaglesDare
#11 Posted : 2/9/2014 7:49:18 PM
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Earthwalker wrote:
WhereEaglesDare wrote:
Thanks everyone, I am in UK so looking for vials. Just worried foil might react in the short term. I though about making paper wraps (like cocaine) and putting in those then in baggies in an airtight jar.


Careful I wrapped some in a cigaret paper once only to have it melt or soak into the paper , so be careful and make sure you're paper isn't absorbent in any way !!


So would foil be ok then? Until I get the vials through.
 
Earthwalker
#12 Posted : 2/9/2014 7:51:53 PM

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I'm sorry but I wouldn't have the experience to say !! But I'm sure the more mature members will know !!
 
WhereEaglesDare
#13 Posted : 2/9/2014 8:20:00 PM
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No worries mate.

Does anyone else know if it reacts with foil?
 
User1911
#14 Posted : 2/9/2014 8:29:58 PM

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Looks good... A better way to store it, if no bottles are available is my simple storing tek , also, vials work good but I find jyarz to be even better. Their air tight, and have a wide mouth opening so you can easily get your dose out. Your yield looks fine to smoke as is. Well done.

If you use baggies some will stick to the sides be lost. As for will it react, I am not sure but a peice of wax paper will solve your problem.
 
WhereEaglesDare
#15 Posted : 2/9/2014 8:49:09 PM
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User1911 wrote:
Looks good... A better way to store it, if no bottles are available is my simple storing tek , also, vials work good but I find jyarz to be even better. Their air tight, and have a wide mouth opening so you can easily get your dose out. Your yield looks fine to smoke as is. Well done.

If you use baggies some will stick to the sides be lost. As for will it react, I am not sure but a peice of wax paper will solve your problem.


That's not all the yield, I have some in a Pyrex jug that looks like yellow goo. It's like oil, no way I can store it as is so will see of a re-x makes any difference.
 
User1911
#16 Posted : 2/9/2014 8:55:27 PM

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well the mhrb goo will harden in the freezer and is smokeable. You can put the goo in with the xtals you have,or keep it seperate. put it in the freezer for a few hours it hardens, then just crush it up and there you go. Youll have dark brown powder.

As for it being yellow oil that may be saturated solvent so be careful with that. Brown goo is more normal.
 
WhereEaglesDare
#17 Posted : 2/12/2014 1:13:03 PM
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I got hardly any yield from the jug/goo so just left abandoned it.

I have tried the crystals and they smoke well, no harshness so no impurities I am guessing.

Is there any difference between the crystals ans brown goo (which I have hardened but gets sticky again at room temp)) in terms of "pureness" or strength?
 
Earthwalker
#18 Posted : 2/12/2014 2:16:37 PM

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Give the goo a go , goo is good !!!Big grin
 
DoingKermit
#19 Posted : 2/12/2014 2:50:22 PM

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Maybe try recrystallising the goo to clean it up a bit. Since you were using MHRB, you would probably get some crystals as a result.
 
V1rusH0st
#20 Posted : 2/12/2014 3:00:37 PM

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Nice work! Beautiful.

That's such a bigger yield than I got from my first MHRB extraction. I am obviously doing something wrong.
 
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