I am wondering about the variables of root bark and it's effecting result on extraction yields.
Factors like age of tree, time of year harvested, section of root selected. Do these greatly effect the extraction
yields?
I ordered 5lbs (2,200g -ish) of ACRB from Hawaii out of this is have only liberated 4 or 5 grams.
Of this i believe the majority has been NMT. ( because of weaker effect and amount of oils present).
I aM THINKING that my source material is lacking. I think that this bark is maybe not Confusa or has a
very low alkaloid content. I understand 100g bark should roughly yield 1g. Is this accurate-(ish) ????
I have been A/B extracting as follows:
Bark- ACRB ( I prepared it to power from whole pieces)
Acid- HCL @ pH 3 for 1 hour (x3) w/distilled h2O (ending w/ 800ml from 400g ACRB)
Filtered- 3x with decreasing porosity filters
Defat- 3x w/ 20% of 800ml about 160ml (1st w/ turpentine) (2nd w/ Zylene) (3rd w/ Naphtha)
Base- Potassium Hydroxide ( based to pH 12.5)
Extract- 3x w/Naptha -(used 100ml per 250g bark) roughly
( for about the first 1000g of the extractions i did not polar wash after extraction)
( the remaining extractions is did water wash until water was clear) about 4 washes with H20 at pH 8.5
I then froze precip. mostly.
I am at i loss as to why i have only recovered about 5g out of 2000g of bark>
Also the effects of the product have been mild..?
Note i did do one extraction using Xylene and let it evap via room temp air ( about 5 days )
it is at the level im looking for if one takes 2 tokes.
I read that NMT is not soluble in Xylene. So far it seems correct. The product is far more potent via it.
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