I was doing Cyb's Tek, skipping the acidifying step, doing heated pulls. I did 2 pulls then put the mixture away in a cabinet and came back to it 3 days later and put more naphtha in it to do more pulls. I also accidentally left the mix on a heated stove and the mixture nearly got to boiling.

Now the naphtha does not seem to be seperating after hours of mixing it up again.

I got like like .8 grams from 2 pulls of 73g of root bark so I'm pretty happy with how much I got but I got 2% yield last time so if it's not fucked at this point I could probably get a good bit more.

Anything I can do to fix or did I waste the rest I could've gotten?

Are you sure the naphta isn't just vaporized because of the heat?

Are you using an airtight container?

Perhaps a lot of the DMT turned into DMT-n-oxide , in that case you might have trouble extracting with naphta. Otherwise, i don't see why you can't just proceed with new fresh naphta.

Possibly, but I think the jar that was sitting in the water was airtight. Nothing would spill when I would shake it, at least. I'll try throwing in another 50ml of naphtha tomorrow and give it another go. If the Naphtha evaporated is that basically a wasted pull?

If the naphtha evaporated the DMT would stay behind.

Something similar happened to me so i threw in another 50 ml. I ended up with what looked like the 50 i threw in plus the first lot that seemed to be missing!

Let me know if this happens to you as i would be interested if this happens to you also.