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Switching Non-Polar Solvent Mid-Extraction? Options
 
oldsoul
#1 Posted : 5/17/2013 6:53:41 PM

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Hello Everyone! Happy Friday Smile

Quick question - I'm in the process of my first extractions, and a small amount of naphtha from the first pulls remains in my extraction vessel (20-30ml). Can I switch to d-limo at this point?

Would the presence of any naphtha cause problems when using FASx for the remainder of extraction? Still haven't decided on FASW or FASI - is there any clear advantage if I have both fumaric acid & 99% IPA?

I was leaning towards FASW since the fumarates will already be dissolved in h2O and ready to convert to fb with sodium carbonate, but not sure if this is practical.

Thanks!!!

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