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The first pull - yellow tint in naphtha Options
 
manyc
#1 Posted : 3/11/2009 3:47:09 AM
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After 3-4 hours of the powdered MHRB soaking in the basic solution (in a wine jug), two of those hours having had naphtha in the solution which was mixed by gently rolling, I siphoned off 250 mL of naphtha (the last bit of it was just too much of a bitch) and it had a yellowish tint. I put it in a huge glass baking pan to evaporate over night in a shed with 3 windows - all opened for ventilation.

I'm guessing this yellowish tint is a good thing? I can only assume that it is. I'm really hoping that in the morning I'll have a small field of crystals awaiting me. Shocked
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weissewolf
#2 Posted : 3/11/2009 4:05:52 AM
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Swim is still pretty new too but he noticed yellow tint usually ends up slightly more dirty on freeze precip.
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appelseen
#3 Posted : 3/11/2009 8:46:30 AM

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Another new SWIM has found out that the longer he lets naphta remain with the solution, the yellower it gets.
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DarkShaman
#4 Posted : 3/11/2009 8:34:47 PM

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appelseen wrote:
Another new SWIM has found out that the longer he lets naphta remain with the solution, the yellower it gets.


This is quite true.

manyc wrote:
I'm guessing this yellowish tint is a good thing?


Not necessarily.

It really doesn't take long to extract each pull (esp. if one uses warm-hot solvents). I usually only leave my solvents in for 30-45 min. per pull, mixing 3-4 times during this time period. I acquire the majority of the alkaloids in this manner, most of which will freeze precip. to beautiful snow-white crystals. I must mention, however, that the degree of "yellowness" achieved will vary in preference to the extractor, as some prefer the "jungleness" of the yellow (other oils & alkaloids that can be found in mhrb besides dimethyltryptamine).

Additionally, I have found it to be harder to reuse "yellowed" solvents. I just save my yellows for the xylene to pick up.
 
mugwump77
#5 Posted : 3/12/2009 12:09:06 AM

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i for one am very much looking forward to hearing how SWImanyc's first time went.
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Dorge
#6 Posted : 3/12/2009 12:24:44 AM

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DarkShaman wrote:
appelseen wrote:
Another new SWIM has found out that the longer he lets naphta remain with the solution, the yellower it gets.


This is quite true.

manyc wrote:
I'm guessing this yellowish tint is a good thing?


Not necessarily.

It really doesn't take long to extract each pull (esp. if one uses warm-hot solvents). I usually only leave my solvents in for 30-45 min. per pull, mixing 3-4 times during this time period. I acquire the majority of the alkaloids in this manner, most of which will freeze precip. to beautiful snow-white crystals. I must mention, however, that the degree of "yellowness" achieved will vary in preference to the extractor, as some prefer the "jungleness" of the yellow (other oils & alkaloids that can be found in mhrb besides dimethyltryptamine).

Additionally, I have found it to be harder to reuse "yellowed" solvents. I just save my yellows for the xylene to pick up.



This is Swims experience as well... Swim also think that using recycled Naphtha will make this more of a possibility as well.

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manyc
#7 Posted : 3/22/2009 12:14:35 AM
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I evaporated that amount of naphtha (haven't tried freeze precipitating yet, though I'd like to) and was left with what must have been at least a gram of snow-white crystals. The smell is unlike anything else I've ever encountered in my life... especially once it's been smoked/vaporized. Though, I can't say that smell is EXACTLY like burning plastic as most people say. It did slightly, but... not exactly.

I'm posting my experience in the appropriate place.

All I will say now, is that never have I experienced such extreme shifts in consciousness, or seen such beautiful displays of colors and impossible shapes. And never, EVER, have I felt that there is something beyond this mundane physical reality where non-physical entities reside.

I do not regret this endeavor at all.
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Hemp can save the World.

Know Thyself.


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