I did a 1 lb. extraction STB style in a one gallon jug. First pull came out dark yellow and subsequent pulls all were a dark brown sludge. We've tried to get it to separate with salt and adding more lye but nothing happened.
We tried a recrystallization and the brown was still everywhere (both with naphtha and heptane). We tried adding 500mL of basified water to the solution and now the water and the naphtha layers are a dark muddy color. What is wrong? Is there anyway to get these layers to separate?
This is a picture of the naphtha recrystallization attempt with about 430 ML of basified water.
