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can this be recrystallized? Options
 
lewinii
#1 Posted : 8/13/2012 4:07:59 PM

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hi everyone.
i just finished a 200gram MHRB STB extraction, and got a decent yield [see picture 1]


there are mostly white crystals there however there is some yellow ones there on the plate as shown on the right hand side of the pic. maybe if i had to fan pre-evap this before i freeze precip the yellow goo might of been much less?

i then went ahead and scraped up all the crystals i could and put them onto a glass plate, and i noticed there was some yellow goo left there in the dish, didnt seem like much so i decided it would be ok to throw it into my pile of white powder. then the powder all turned into yellow clumps. lol :/

so this is now what i have..[see picture 2]


not sure the weight of this, but im guessing about 2 grams. i dont have a accurate enough scales yet.

i wanted to know, is this ok to re-x? i dont know if my dmt is now dmt-oxide..
wanted to try this guide https://www.dmt-nexus.me....aspx?g=posts&t=1266

thanks for your time,
lewinii attached the following image(s):
picture-1.jpg (146kb) downloaded 125 time(s).
picture-2.jpg (93kb) downloaded 124 time(s).
"science never proves anything; you can never duplicate an event precisely at the same moment in time as the initial event. science can only show correlation from the evidence and data derived from it." -benzyme

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3rdI
#2 Posted : 8/13/2012 4:12:50 PM

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it will be fine for re-X
INHALE, SURVIVE, ADAPT

it's all in your mind, but what's your mind???

fool of the year

 
lewinii
#3 Posted : 8/13/2012 5:30:01 PM

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thanks 3rdI for the reply. i will re-x as soon as i got the time to do it!
"science never proves anything; you can never duplicate an event precisely at the same moment in time as the initial event. science can only show correlation from the evidence and data derived from it." -benzyme

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3rdI
#4 Posted : 8/13/2012 5:30:44 PM

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Thumbs up take a pic and show us your lovely crystals
INHALE, SURVIVE, ADAPT

it's all in your mind, but what's your mind???

fool of the year

 
wearepeople
#5 Posted : 8/13/2012 8:04:19 PM

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Maybe check out Vovin's tek and look at the "washing" section.

Recommend dissolve product in Naptha (300mL).
Then, pinch of sodium carbonate in about 100mL distilled H2O.
Mix the two, shake vigorously (very quick separation).
Separatory Funnel.

Repeat twice more but without adding Sodium Carbonate.

Then Re-x.

Find this helps provide dry crystals from Freeze Percip.
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lewinii
#6 Posted : 8/13/2012 10:23:41 PM

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before i froze the dish, i had done 4 vigorous pulls of 75ml each, so 300ml naphtha.

after there was 150-160ml.. so about half of it evaped away
i kept the leftover naphtha for now
"science never proves anything; you can never duplicate an event precisely at the same moment in time as the initial event. science can only show correlation from the evidence and data derived from it." -benzyme

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lewinii
#7 Posted : 8/13/2012 10:54:08 PM

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yup after the freeze precip, i put my dish into a small cardboard box along with a small fan.. closed the box up and left it alone for awhile. maybe i should have left the dish dry longer and that yellow goo could have been crystals instead. not sure why yours turned to goo after a fan dry.. maybe it oxidized?
"science never proves anything; you can never duplicate an event precisely at the same moment in time as the initial event. science can only show correlation from the evidence and data derived from it." -benzyme

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wearepeople
#8 Posted : 8/13/2012 11:38:47 PM

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Maybe check out page 10 of "The DMT Handbook".

It explains a method of freeze precipitation where the globe is turned upside down and quickly placed back in the freezer to let the remaining Naptha drain off.
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lewinii
#9 Posted : 8/15/2012 5:05:17 PM

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just wanted to come back and show my results.. i was skeptic at first that maybe i lost a lot more crystals than 10%, because in the dish they looked so much smaller. however, i think these are more compacted because i didnt lose near as much as i thought i would.

they came out basically pure white, really happy with this, i will keep this spice in a different container because its so pure. and i could see the leftover gunk in the shot glass, glad thats out of my spice
lewinii attached the following image(s):
1-2.jpg (117kb) downloaded 95 time(s).
3-4.jpg (92kb) downloaded 96 time(s).
"science never proves anything; you can never duplicate an event precisely at the same moment in time as the initial event. science can only show correlation from the evidence and data derived from it." -benzyme

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Ice House
#10 Posted : 8/15/2012 5:31:12 PM

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Nicely done!
Ice House is an alter ego. The threads, postings, replys, statements, stories, and private messages made by Ice House are 100% unadulterated Bull Shit. Every aspect of the Username Ice House is pure fiction. Any likeness to SWIM or any real person is purely coincidental. The creator of Ice House does not condone or participate in any illicit activity what so ever. The makebelieve character known as Ice House is owned and operated by SWIM and should not be used without SWIM's expressed written consent.
 
Korey
#11 Posted : 8/15/2012 5:35:58 PM

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Nice job, man! Razz
“The most compelling insight of that day was that this awesome recall had been brought about by a fraction of a gram of a white solid, but that in no way whatsoever could it be argued that these memories had been contained within the white solid. Everything I had recognized came from the depths of my memory and my psyche. I understood that our entire universe is contained in the mind and the spirit. We may choose not to find access to it, we may even deny its existence, but it is indeed there inside us, and there are chemicals that can catalyze its availability.”
 
 
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