I really did search this question the best I could with this search engine, and didn't find a definitive answer. So here goes:
Ok, so now I'm finally doing an A/B on MH powder, and so far, what I've done is, put 50 g of MH into a glass jug and then put 250 ml of white vinegar (that is somewhat old but definitely still acidic) in too, and that's been in my warm garage (about 85 F) overnight now. After a while, I'll add water in the right proportions (actually, I'm using more vinegar by proportion than the usual teks call for, to make SURE it's of high enough acidity) to this solution and simmer it on the stove for 1.5-2 hours, let the sludge settle, decant and repeat with smaller amounts of vinegar/water, twice. (I'll have to use more lye to basify than marsofold's tek requires, I know).
Question:
After that's done and the sludge has settled, what should the solution above the sludge look like? Right now the sludge keeps falling to the bottom and a vinegar/whatever else solution which is basically black is on top (again it's nothing but 50 g MH powder + 250 ml white vinegar).