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Re-wrote Q21Q21 Tek1 combined with BLAB 4b. Need confirmation. Options
 
purple_dye
#1 Posted : 5/2/2012 5:21:47 PM

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I re-wrote this Tek (with some minor tweaking)to meet my understanding and flow and just want to make sure that what I'm about to do will work.

There are specific reasons I decided to do the tek this way instead of the normal naphtha version. Mainly I don't have a freezer. Also, even though I'm scientifically minded enough to realize that using conventional chemicals is just as safe as using food grade... I just am in love with the notion of being as natural as possible.

Positive criticism is welcome. Ive had countless Aya experiences and have finally decided its time to smoalk. Razz

Supplies:

• 50g MHRB
• 50ml 5% white vinegar
• Large glass container
• Distilled water
• Wood chop stick or something similar to stir
• 50g lime
• 375-500ml d-limonene
• HDPE2 milk jug
• 2 funnels
• Cotton balls
• 2 mason jars
• fumaric acid
• sodium carbonate


TEK

1. Place 50g MHRB large glass container

2. Add roughly 50ml 5% white vinegar to container until most of bark is wet, red, and clumpy

3. While stirring, slowly add about 50ml of near boiling distilled water. Add until it is wet enough to allow for flow when the container is tipped from one side to another. The bark will absorb some of the water the first few minutes. Add more warm/hot water to get it wet enough again as needed.

4. Stir several times as the bark is left to sit for 45 minutes (stir periodically)

5. Add 40g-50g lime to mix bit by bit and mix in well.

6. Add water (if needed) to make the mix look anywhere from thick oatmeal to a thick pea soup.

a. If too dry add water (small amount at a time)
b. If too wet add lime

7. Add 75-100ml d-limonene

8. Stir or roll periodically over next 24 hours

9. Pour solvent from bark into HDPE2 milk jug through a funnel with a cotton ball. You needn't be too fussy about getting 100% of the solvent. Pouring usually gets 90% or more.

10. Repeat steps 7-9 at 2 days 4 days 7 days and 14 days.

11. Fill a mason glass jar with water and add a teaspoon of fumaric acid to it while mixing strongly for a minute or two. Add more slowly until undissolved material falls to the bottom.

12. Decant this jar so only FASW (fumaric acid saturated water) solution is left.

13. Mix limonene pull with FASW solution in a ratio of 5:1 (5 parts limonene to 1 part FASW solution)

14. Mix well and let layers separate and pull FASW out.

15. Repeat steps 15 and 16 2 more times putting all FASW in same container

16. Let FASW evaporate. You now have DMT fumarate which can be taken orally with a MAOI but not smoked.

17. Make a small amount of saturated sodium carbonate solution by adding sodium carbonate to water until no more will dissolve.

18. Decant sodium carbonate saturated solution to remove precipitate

19. Add just enough near boiling water to glass container holding dry dmt fumarate until completely dissolved.

20. Slowly add a small amount of sodium carbonate saturated solution to dmt fumarate solution only a few Ml at a time. Let rest a few minutes and add a few more Ml. Keep adding until no more clouding or color change occurs and then add a little more for good measure. GO SLOW.

21. Put container into fridge for 3-5 days and dmt crystals will precipitate out completely

22. Pour off water though a coffee filter

23. Scrap up dmt from bottom and let dry

24. Smoalk DMT freebase

PS

This is what the alphabet would look like if Q and R were missing
 

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Pup Tentacle
#2 Posted : 5/2/2012 5:48:08 PM

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sweet... I'm currently working on something similar...
Pup Tentacle

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dreamer042
#3 Posted : 5/2/2012 8:59:46 PM

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This tek should work fine Thumbs up
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Visual diagram for the administration of dimethyltryptamine

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Organicosis
#4 Posted : 4/28/2013 10:59:06 PM
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I know this is an old thread but instead of starting a new one i'd like to ask here. This shouldn't be any different for acacia confusa right? This sounds like a spectacular tek, anything all natural is great.

Also another thing I might try another way and use naptha to see if crystals crash out in room temp like in thick-lights tek. I've read on the shroomery freeze precip doesn't work, but that dissolving the goo in isopropyl alcohol and leaving to evaporate results in crystals, in any case I'm going to figure something out. Can anyone give me any good advise?
 
Organicosis
#5 Posted : 4/29/2013 2:06:04 AM
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*Bump* d limonene is all I can get, I don't want to mess with naphtha anyways. I guess I can try it to see what happens first, since I've read the alkaloids can always be recovered. Anyone try this with A. Confusa though? Will the Nmt stop the dmt from precipitating in water? I read in the wiki Nmt freebase is the goo.
 
Parshvik Chintan
#6 Posted : 4/29/2013 7:20:27 AM

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even DMT from sources with no NMT (such as MHRB) comes out gooey (but that's ok). both the NMT and DMT will precip into the water, as alkaloids are wont to do.

one thing i will say is that it is been shown that using hdpe2 plastic with limonene is probably not a good idea (we are fairly sure the limo leaches some plasticizers, we aren't sure if they end up in the product, if they are harmful, or if they are plentiful).

other than that, this tek will work fine for acacia.

also, when i did my Q21Q21 tek, rather than just adding hot water and letting sit, i put the glass container in the oven at 200ºF for a good 45 mins (making sure it stayed hydrated). and i vigorously stirred the limo with the bark-paste (using a metal spoon) until the originally clear limonene turned from yellow to orangey-red (the resulting jim-jam was blood red).

as you are extracting a different species, the color change may not be identical (or as noticeable).
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Organicosis
#7 Posted : 5/3/2013 12:22:14 AM
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Hey thanks P. Chintan! Appreciate the tips.
 
 
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