Hello all just wanted to stop off and say hi.
swim has been cruising your forums for a while and wanted to thank everyone who has provided such quality information on spice and obtaining it.
as of right now swim's MHRB shows up today and will start their first extraction using a STB method. it seams straight forward and hope to have good results; will keep everyone informed on how it goes.
swim only concern is after ordering all the materials and getting new glass etc, found out yay the environment and out air quality control, cant get vm+p naphtha in this area so swum had to get Colman camp fuel as recommended by others. well hoping that, that does not cause an issue like green spice but swim's understanding is worse case scenario just re-x? (please correct me if i am wrong)
Swim just finished making sodium carbonate out of bicarb to do a carbonate wash. (baking soda in a pan on high, until the reaction stops.)
so basically the plan is
NAOH + H20 let reaction stop.
add MHRB. let set up for an hour
add fuel. mix gently to avoid emulsifying.
let separate and decant
collect pulls.
take collected fuel layers and add wash (h20 + sodium carbonate)
shake and let separate.
decant 1 more time and evap fuel in a large flat dish.
repeat
after its all dried hope to have some nice crystals. but if not re-x.
please if swim missed anything or anyone had input please let me know.
as for freeze precipitation i may see if i can get a freezer to use. but as of now swim cant turn the freezer down low enough. and more so swim roommate prob wouldn't like his son asking what the jars of spice in the freezer are for. lol (fyi any cooking or traveling is not done with the child in the house)
swim pre apologizes if he shouldn't have gone over any of this in this forum but swim is very excited about his first chem project and wants to make sure he does it right.