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analoge
#1 Posted : 8/29/2011 12:01:35 AM

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Embarrased
 

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endlessness
#2 Posted : 8/29/2011 12:05:05 AM

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I would avoid defatting and go for FASA on xylene (yuck) or FASI on limonene (nomnom). defatting is a very wasteful process, unless you can distill your solvents. Fumarate precipitation bypasses the need of defatting because the alkaloids precipitate directly and the fats/oils remain dissolved in the solvent. Then after decanting/filtering your crystals, you wash them with cold dry acetone or ipa to remove limo/xylene traces and any potential excess fumaric acid, and then you convert it to freebase by crystallizing out of water with sodium carb as mentioned in BLAB.
 
analoge
#3 Posted : 8/31/2011 11:22:38 PM

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Embarrased Dum nah the salts would need water to be transferred into so that was a dum idea I would wash away the goodies

I wont try it
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