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are lots of small pulls better than one big pull Options
 
buk
#1 Posted : 8/18/2011 10:34:16 PM

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Swim has always done small pulls with naptha of about 50ml but the marsofold tek suggest just doing one 300ml pull.

Is there a difference?

with a 500g extraction is 300ml reccomended? and what amount is best to evap it down to before freeze precip?

thanks,
 

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#2 Posted : 8/18/2011 10:41:46 PM

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I would stick with 50 or even 90 (90 is 3 shots), 300 seems like overkill,
pull until you do not notice the solvent changing colors, then combine and evaporate to at least half the original volume.... then freeze precip.
 
Xt
#3 Posted : 8/18/2011 11:31:33 PM

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To answer the question
Quote:
are lots of small pulls better than one big pull

Yes.

Magic info:
For an STB
0.4ml naphtha per gram of bark, per pull.
Five pulls is ideal.
Thus for a 100g bark extraction... 100 x 0.4ml = 40ml per pull.
40ml x 5 = 200ml total.


Do the pulls, combine total pulls, evaporate to 50% volume (outside), then freeze precipitate.

β€œRight here and now, one quanta away, there is raging a universe of active intelligence that is transhuman, hyperdimensional, and extremely alien... What is driving religious feeling today is a wish for contact with this other universe.”
― Terence McKenna
 
soulfood
#4 Posted : 8/18/2011 11:36:37 PM

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I do one big pull.

The things is if you're going to do one big pull, you have to really mean it. I use 1-200ml and I agitate hard and often for days. Then I heat the last time I agitate and separate damn quickly...

Then cool damn slowly Smile

Also when doing an STB there's no point doing this unless the bark's been soaking for at least 2 days.
 
Xt
#5 Posted : 8/18/2011 11:40:49 PM

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According to this cat, there are many ways to remove his permeable organic barrier.

β€œRight here and now, one quanta away, there is raging a universe of active intelligence that is transhuman, hyperdimensional, and extremely alien... What is driving religious feeling today is a wish for contact with this other universe.”
― Terence McKenna
 
endlessness
#6 Posted : 8/19/2011 12:41:39 AM

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buk
#7 Posted : 8/19/2011 2:18:12 PM

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Thanks for all the info. Sorry should have checked the faq.
 
 
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