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Acacia Confusa Extraction On The Go, Few Questions Options
 
endlessness
#21 Posted : 3/23/2011 9:36:55 AM

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yeah as he said ^


By the way if you are adding all the pulls together, its possible the later pulls are not as saturated with dmt as the first, so maybe not all (or not most) of your dmt will crash out during freeze precip, maybe you should evaporate the naphtha a bit (like lets say till half) and put in the freezer, or at least be sure to reuse the naphtha after retrieving the crystals.
 

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toppy
#22 Posted : 3/23/2011 7:03:51 PM

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Ok there were loads of crystals at the bottom of my dish, but EVERY white crystal melted when exposed to the air, even after the dish was upside down in the freezer, but i do think this is because the naptha wasnt dropping off the bottom properly due to its design, so i took all the naptha out and scrapped all the yellow crystals which did not melt, theres roughly 70-80mg of yellow crystals, i evaporated them dry and dabbed a tiny bit on my tongue, it was like a burning plasticy sensation which numbed my tongue for about 20 mins. Im not going to recrystallize these, going to do a dose of a third of the weight.

There was about 4-5x as much white crystals as there was yellow, i emptied the npatha from the dish into a new jar and put the empty dish back into the freezer on its side, it seems the white crystals are forming again and the leftover naptha is dripping off now. I also put the jar with the naptha in the freezer to.

From this first extraction i have learned alot and have a much better understanding of the science behind how it all works, next time i will be better prepared with better equipment.

Im having trouble with a camera but i will post some pictures of the white crystals when i have "mastered" the process.
 
fourthripley
#23 Posted : 3/23/2011 9:29:08 PM
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This Edot thread may be of interest hxxp://www.entheogen.com/forum/showthread.php?t=26872
mistakes were made
 
DoingKermit
#24 Posted : 3/24/2011 2:00:30 PM

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I am looking forward to seeing some pics. I really need to order some bark and try do an A/B on it. Thanks again toppy
 
toppy
#25 Posted : 3/24/2011 2:47:18 PM

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The white crystals wont stop melting when exposed to the air, i even froze a jar with just the melted DMT in it, and got a nice big silky white crystal, but after 10 minutes it starts to melt again, im not sure if this is a freezer problem but its doing my head in a bit.
I smoked the yellow crystals and half experienced what i getting into, but it was quite harsh and hard to keep in my lungs or inhale to much. Saw nice geometric patterns, diamonds colors etc for about 20 seconds, felt like i was inside of a sphere, until i got distracted by some white light and i opened my eyes and couldnt get back. I really need to get these purer crystals to solidify.
 
DoingKermit
#26 Posted : 3/24/2011 5:10:02 PM

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I suggest placing your jar upside down in the freezer for a couple hours and when you take it out, unscrew the lid keeping the jar upside-down. Then take a paper towel and wipe the inside lip of the jar so the last of the solvent doesn't drip back into your crystals. Take a fan and keep it over the jar for over an hour to make sure all your solvent has evaporated. The crystals hopefully won't melt or dissolve.
 
soulfood
#27 Posted : 4/1/2011 4:16:08 PM

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I just ground up a whole load of this plant in my coffee grinder.

It left a gummy residue on the top of the cover, so my intuition is telling me a defat is more than likely quite necassary to get good results from this material.
 
DoingKermit
#28 Posted : 4/1/2011 4:22:43 PM

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I figured an A/B would most likely be the better choice. Let us know how it goes, soulfood
 
Ljosalfar
#29 Posted : 4/1/2011 4:35:05 PM

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Soulfood... smoke the gummy, just to see?
A long shot, but worth a try.
L
"The first principle is that you must not fool yourself, and you are the easiest person to fool." Richard P. Feynman
 
soulfood
#30 Posted : 4/1/2011 4:42:10 PM

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Ljosalfar wrote:
Soulfood... smoke the gummy, just to see?
A long shot, but worth a try.
L


A very long shot...

and no. I value my lungs. Smile

But I could do a small extraction on the gum. Dissolve in actone, then add FASA maybe?

I'd bet on it being 95% plant oils though.
 
acolon_5
#31 Posted : 4/1/2011 4:49:07 PM

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toppy wrote:
The white crystals wont stop melting when exposed to the air, i even froze a jar with just the melted DMT in it, and got a nice big silky white crystal, but after 10 minutes it starts to melt again, im not sure if this is a freezer problem but its doing my head in a bit.
I smoked the yellow crystals and half experienced what i getting into, but it was quite harsh and hard to keep in my lungs or inhale to much. Saw nice geometric patterns, diamonds colors etc for about 20 seconds, felt like i was inside of a sphere, until i got distracted by some white light and i opened my eyes and couldnt get back. I really need to get these purer crystals to solidify.



I'm reading that a simple recrystalization will stop the melting xtal problem.

Do we know what temp NMT melts at?
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