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Residue left in solvent Options
 
FusionOracle
#1 Posted : 12/5/2010 3:06:50 AM

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SWIM has just completed an extraction - following the DMT handbook tek, using warm shellite for solvent (he also used quite a bit of solvent for his pulls as he was finding it hard to pull with little in there - he plans to evap before freeze percip).

After pulling the solvent it was left in a bottle to decant for half an hour (SWIM was using a turkey baster and as such some of the solution was pulled up with the solvent).

After it had decanted in the bottle he carefully poured off the solvent into a glass, none of the solution which was sitting at the bottom was allowed to enter the glass. The solvent in the glass was a nice milky colour with a yellow tinge (from what he has read this is a good sign?????)

He left the solvent in the glass over night and when he returned to it the next day he poored it into a glass bowl to do some evap before freeze perip. He noticed that the milky colour had subsided and the solvent was now more of a transparent yellow colour.

He then noticed that stuck to the bottom of the glass there was a thin layer of what appeared to be little white xtals but upon closer inspection they seem to be condensed droplets. He used a spoon to see if he could scrape them up and found that they turned to a yellowy, dark orange oily type liquid when agitated.

SWIM is wondering what this is - whether it is impurities left over from the solution that was suspended in a very small quantity in the solvent (as the colour once agitated resembled this) or whether this is spice?????

Should he dissolve in hot naptha and freeze percip or simply discard????



Update: SWIM has attempted to redissolve in hot naptha but the oil/goo stays and the bottom of the glass and is not absorbed.

He is now thinking that these could be a small amount of oils/fats from the MHRB powder???? Or could this be jungle as previously mentioned??????

Can anyone help clarify???

Would it be safe to attempt a taste test if it is dried????

Note: the residue smells of spice?????????
 

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biopsylo
#2 Posted : 12/5/2010 5:29:05 AM

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if swiy used warm, or hot shellite, then perhaps this is pulling some "jungle". or it could also be water that came over, and collected on the bottom. either way, noting that swiy is using shellite, and not xylene or linonene, then white crystals are preferred? if this is the case, maybe best to discard.
 
Eranik
#3 Posted : 12/5/2010 4:22:17 PM

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If you're absolutely sure none of the water was pulled along your solvent, then it is n-oxide DMT or NMT if i'm not wrong, which is active itself, don't discard. keep that, you can either smoke it later as it is or convert it to DMT using zinc dust.
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FusionOracle
#4 Posted : 12/5/2010 9:23:44 PM

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Thanks.

SWiM is now pretty sure it's N-oxide DMT. Is there any way to stop this reaction occurring until SWIM freeze percips???
 
justine
#5 Posted : 12/5/2010 11:08:39 PM

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Eranik wrote:
If you're absolutely sure none of the water was pulled along your solvent, then it is n-oxide DMT or NMT if i'm not wrong, which is active itself, don't discard. keep that, you can either smoke it later as it is or convert it to DMT using zinc dust.


NMT stands for methyltryptamine and isn't dmt n-oxide.
To see the world in a grain of sand, and to see heaven in a wild flower, hold infinity in the palm of your hands, and eternity in an hour.
- William Blake
 
justine
#6 Posted : 12/5/2010 11:10:30 PM

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FusionOracle wrote:
Thanks.

SWiM is now pretty sure it's N-oxide DMT. Is there any way to stop this reaction occurring until SWIM freeze percips???


If it's n-oxide it was most probably extracted directly from your mimosa soup and it doesn't come from oxidation of the dmt in your solvent.
To see the world in a grain of sand, and to see heaven in a wild flower, hold infinity in the palm of your hands, and eternity in an hour.
- William Blake
 
FusionOracle
#7 Posted : 12/6/2010 6:59:39 AM

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SWIM has done some reading and is now not sure whether it is n-oxide, oils/fats from the MHRB or other active substances.

He attached a picture. Can anySWIY take a look and give him their opinion on; what it is, is it safe and what’s best to do with it?????

Thanks.
FusionOracle attached the following image(s):
IMG_4394.JPG (2,724kb) downloaded 38 time(s).
 
 
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