Arthur
Posts: 41 Joined: 10-Jan-2010 Last visit: 16-Sep-2011 Location: the Here'n'now
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i used 150g of MHRB in a solution of 150g lye and 3000ml water and 50 ml naptha for this pull (the bark was prepowdered) and im using normans tek i have just completed my first naptha pull (though it hasnt been frozen yet) I agitated 6 times allowing a 1-2 minutes for agitation, and then a full seperation afterwards. my naptha hasnt come out cloudy, does this mean i need to reduce the naptha in my pulls? Thanks Joy I is someone else
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DMT-Nexus member
Posts: 728 Joined: 09-Oct-2009 Last visit: 01-Jan-2022 Location: London
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No, all sounds good to me. Do 5 or 6 pulls, combine them then freeze precip. Oh great - the world has just been replaced by elf machinery.
Sic transit gloria mundi
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DMT-Nexus member
Posts: 2807 Joined: 19-May-2009 Last visit: 16-Mar-2024
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do as ^ says, and then evap till it gets cloudy, then freeze, this way the naptha is nice and saturated and the Spice will crash out nicely when in the freezer. When you get to the last few pulls i would leave in for a longer period, with an aggitation here and there.
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DMT-Nexus member
Posts: 105 Joined: 21-May-2010 Last visit: 18-Feb-2019
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ah so is it reccomended to do all the pulls and then combine before the freeze precip? How much naptha do you reccomend per pull ?
Whats the agitation step mentioned above swim hasnt heard of this.
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DMT-Nexus member
Posts: 15 Joined: 12-Jun-2010 Last visit: 02-Feb-2011
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Your naphtha will get cloudy when it FREEZES. At warm temperatures, it should be slightly yellow/orange and clear.
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DMT-Nexus member
Posts: 582 Joined: 11-Jun-2010 Last visit: 23-Sep-2013 Location: that warm fuzzy place... hyperspace
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i always pull half of my total solvent. freeze precip and poor off the solvent back into my extraction jar. keep goin until you dont get anything. -Close your eyes, See the light, and feel the sunshine in the shade
~All views, ideas and opinions of this user are strictly fictional and in no way represent an act done in reality.
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Arthur
Posts: 41 Joined: 10-Jan-2010 Last visit: 16-Sep-2011 Location: the Here'n'now
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Cool! Well on the way to hyperspace now.  I is someone else
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Arthur
Posts: 41 Joined: 10-Jan-2010 Last visit: 16-Sep-2011 Location: the Here'n'now
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oh yeah, buk its just shaking up the soup when the napthas in its so that the naptha gets to meet the spice thanks for the help guys I is someone else
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DMT-Nexus member
Posts: 105 Joined: 21-May-2010 Last visit: 18-Feb-2019
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oh I see, I thought this was something you were doing after the pull.
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Arthur
Posts: 41 Joined: 10-Jan-2010 Last visit: 16-Sep-2011 Location: the Here'n'now
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Another related side question, if the naptha is a glaring shade of yellow does this mean ive hit the payload, or ust that ive pulled a load of plant oil too? I is someone else
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DMT-Nexus member
Posts: 318 Joined: 21-Oct-2009 Last visit: 15-May-2019
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sleeper wrote:Your naphtha will get cloudy when it FREEZES. At warm temperatures, it should be slightly yellow/orange and clear. The naphtha wont freeze. well at least not in any conventional freezer! ha. thats the whole point! otherwise it wouldn't work very well ;-) No drug, not even alcohol, causes the fundamental ills of society. If we're looking for the source of our troubles, we shouldn't test people for drugs, we should test them for stupidity, ignorance, greed and love of power. ~P.J. O'Rourke
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DMT-Nexus member
Posts: 2807 Joined: 19-May-2009 Last visit: 16-Mar-2024
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glasseyed wrote:Another related side question, if the naptha is a glaring shade of yellow does this mean ive hit the payload, or ust that ive pulled a load of plant oil too? It meant you have lots of oils , immediate cloud formation in the naptha means a good pull was done. Freeze precip.
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DMT-Nexus member
Posts: 557 Joined: 09-Sep-2009 Last visit: 26-Jun-2012
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You have yellow plant oil/fat contams because you just did a STB. An a/b or recys will remove those oils.
Edit: Also for best yields you must evap down the naptha until it goes cloudy. If you don't there is more space for DMT to stay soluble in when the solution is cooled in a freezer for 2-3days, hence not all of the DMT will precipitate out.
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