The longer you let it sit before adding the d-limonene the better the tech works. You'll get higher yields, and mixing will be easier. It takes time for the calcium hydroxide to work.
Your best bet would be to let it sit overnight mixing it once in a while before adding the d-limonene. Anymore would be a waste of time. This gives the calcium hydroxide more time to freebase the alkaloids, and more time to break down the cactus mucilage. The cactus mucilage prevents the alkaloids from being extracted easily, and needs to be broken down. That process takes a while.
One thing I want to mention, don’t use a lot of heat at any part of the process, especially at the end when drying the vinegar solution. Too much heat will destroy the mescaline acetate and give very poor yields. I’m sure you already know that, but others might not, so I wanted to make sure to repeat that here.
You may remember me as 69Ron. I was suspended years ago for selling bunk products under false pretenses. I try to sneak back from time to time under different names, but unfortunately, the moderators of the DMT-Nexus are infinitely smarter than I am.
If you see me at the waterpark, please say hello. I'll be the delusional 50 something in the American flag Speedo, oiling up his monster guns while responding to imaginary requests for selfies from invisible teenage girls.