Dimitrius wrote:bump...
So I'm about to extract from some older chaliponga with the intent of infusing the freebase result into a leaf blend.
Like this: basify with lime > pull with limonene > precipitate with FASI > freebase the fumarates with lime...dry > then pull with dry IPA or acetone
Now I know it works up to the fumarate stage. I've done this to that point before. But what I'm wondering is if I freebase and pull with IPA or acetone, will the result be a 5-MeO-DMT/DMT mixture? Will the 5-MeO be pulled with these solvents?
And if one were to recrystallize with heptane...would the 5-MeO be soluble in heptane?....resulting in a cleaned up 5-MeO-DMT/DMT mixture?
Knowledge & wisdom greatly appreciated.
So....went ahead with the above ^^ procedure....only instead of pulling from the dried paste with IPA or acetone, heptane was used.
Full-spectrum was desired, but a bunch of unknown brown stuff precipitated along with the fumarates...this was obviously to do with the old, low quality leaf....with high quality, fresh leaf, only beautiful fumarates precipitated....so, went with heptane.
Yielded a beautiful golden yellow chaliponga sacrament...it really looked nice
....subsequently infused into blue waterlily petals. Awaiting assay in the right moments.
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