Respecting the plant, getting more Spice - wanting to try Xylene Options
#1 Posted : 6/18/2022 10:49:24 PM
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I've had a pleasant surprise at the purity of the Spice I've extracted with Q21Q21's Vinegar/Lime method. I've only used Naphtha as my non-polar solvent so far and I've seen how it slowly absorbs into the bark mush. Before I try Xylene should I completely dry the bark mush? That is, give the Naphtha a chance to evaporate? Or is it just fine to pour off the excess Naphtha and start stirring in some Xylene?

I'm really interested to see if I can extract something a bit more jungly.

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#2 Posted : 6/19/2022 2:33:12 PM

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Xylene is so effective a solvent that you don't have to worry about the naphtha remnants, unless you have some overarching reason to avoid getting naphtha into your xylene (I can't think of any).

How will you be getting the product back out of the xylene? Evaporation is slow and xylene is really stinky (although I kind of like the smell).

To keep up the 'jungle-ness' a good option might be to backsalt into vinegar, evaporate, base with sodium carbonate, allow the paste to dry and then pull with acetone (or IPA, or ethanol) and evaporate once more. It seems worth mentioning that fumaric acid precipitation would likely clean things up too much.

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