What, swimbo was the first one? Ha!
Swimbo can’t tell the yield cause he’s pulling from a highly concentrated bottle (frozen, pressed material, a lot of it). As a matter of fact he’s still pulling 4g each time. If there ever was a bulk method this ought to be it. Swimbo will try again with 400mg next time. Also he will recruit a fellow pschonaut to make sure its not just him going bonkers. He has definitely had 500mg of HCI b4, nothing like this.
Borderline hyperspace, cartoonland shit…newish territory after 20 years of tripping
It took a while to come on, just as usual, so not a particular fast absorption. He expected threshold effects since that was from a pull that wasn’t even sparkly needle crystals, just white powder. Boy, he was in for a surprise! He tried to ignore the effects initially but had to sit down eventually. There were iridescent metallic looking mandalas. Even pure gold colored stuff. Never seen anything like this before. When swimbo’s buddy showed up he said he couldn’t tell just by looking at him but his brains were hanging out for sure. LOL

Good idea with the hot acetone wash. Swim will try this to reX.

after more people have tried this we should write up a new CITLO tek!

👍🏻

should this be dry acetone for washing?
Can you clean Toluene the same way as EA?

Not sure if needs to be dry acetone. It is less likely to loose any product with dry acetone, so why not. I would use fresh acetone and evaporate to check for any loss of product.

I think so. A sodium carbonate or (for toluene only) NaOH water wash should remove any excess benzoic acid. You can check with a pH strip.

Heya. - Turns out there is a 40% loss when washing with acetone. Methanol and IPA dissolves most everything too. So does EA. No way 40% of this material is bad. Bummer, since there are some of those notorious solvent burbs swim wants to get rid of. Maybe Re-X is a better way to clean it up?