We've Moved! Visit our NEW FORUM to join the latest discussions. This is an archive of our previous conversations...

You can find the login page for the old forum here.
CHATPRIVACYDONATELOGINREGISTER
DMT-Nexus
FAQWIKIHEALTH & SAFETYARTATTITUDEACTIVE TOPICS
Mescaline tartrate Options
 
doubledog
#1 Posted : 1/13/2022 9:56:18 AM

DMT-Nexus member


Posts: 545
Joined: 02-Dec-2017
Last visit: 17-Feb-2024
Location: right side of the river
Trying various acids for salting mescaline I came to tartaric acid. It seems to work quite well, suitable for recrystalization from water/acetone.
I still have to tweak the procedure somehow, as it is clearly visible that crystals are not uniform and pure.

Crystals were precipitated from xylene by addition of tartaric acid dissolved in small amount of ethanol, separated by filtration and re-x from water/ acetone mixture. It is most likely monomescaline tartrate.
doubledog attached the following image(s):
20220112_191744.jpg (1,911kb) downloaded 97 time(s).
 

Live plants. Sustainable, ethically sourced, native American owned.
 
Loveall
#2 Posted : 1/13/2022 10:33:51 AM

❤️‍🔥

Chemical expertSenior Member

Posts: 3648
Joined: 11-Mar-2017
Last visit: 08-Dec-2024
Location: 🌎
Great result 👍

I'll try to add tartaric acid directly to freebase mescaline in ethyl acetate, see if that also creates xtals.

Any reason to suspect it is the monomescaline tartrate form?
💚🌵💚 Mescaline CIELO TEK 💚🌵💚
💚🌳💚DMT salt e-juice HIELO TEK💚🌳💚
💚🍃💚 Salvinorin Chilled Acetone with IPA and Naphtha re-X TEK💚🍃💚
 
doubledog
#3 Posted : 1/13/2022 10:53:28 AM

DMT-Nexus member


Posts: 545
Joined: 02-Dec-2017
Last visit: 17-Feb-2024
Location: right side of the river
Thanks Smile
300 mg of acid was used to obtain 700mg of final product. Not really sure about all the calculations with molecular weights, but this seems quite a lot of acid for relatively small amount of product.
 
Cheelin
#4 Posted : 1/13/2022 5:39:49 PM

DMT-Nexus member


Posts: 465
Joined: 24-Nov-2021
Last visit: 02-Apr-2022
Location: Here
Good work there DD!
 
doubledog
#5 Posted : 1/14/2022 8:11:15 AM

DMT-Nexus member


Posts: 545
Joined: 02-Dec-2017
Last visit: 17-Feb-2024
Location: right side of the river
Same material before recrystalization
doubledog attached the following image(s):
20211215_121434.jpg (1,785kb) downloaded 56 time(s).
 
 
Users browsing this forum
Guest

DMT-Nexus theme created by The Traveler
This page was generated in 0.013 seconds.