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benzyme
#21 Posted : 1/26/2019 3:48:14 PM

analytical chemist

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this is super frustrating....
I changed the operating reservoir fluid (turbomolecular pump oil), and have since been unable to attain adequate vacuum to initialize the ion gauge. Either the ion gauge is bad, or there is a leak. I've been troubleshooting for a week..

I was able to fix an issue with one of my UV detectors, so I'm able to do quantitative work; will be able to do enantiomeric separation as well (determination of isomers in a racemic mixture).

"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
XMR 46JqfBqi7JNM1W5rXXZ1FF1CBKKLoGEVBRya9Cn3RJmPbQhT4GeZpVKWbwaVe4vUMveKAzAiA4j8xgUi29TpKXpm3whx5MW
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Good quality Syrian rue (Peganum harmala) for an incredible price!
 
Loveall
#22 Posted : 1/26/2019 4:55:39 PM

šŸ’–

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Are you able to do a helium leak check?
ā€œ... (a) psychedelic substance occasionally causes psychotic behaviour in people who have not taken it.ā€
Excerpt from a McKenna talk transcript / audio.
 
benzyme
#23 Posted : 1/26/2019 6:12:33 PM

analytical chemist

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possibly, but the helium is shut off at the cylinder.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
XMR 46JqfBqi7JNM1W5rXXZ1FF1CBKKLoGEVBRya9Cn3RJmPbQhT4GeZpVKWbwaVe4vUMveKAzAiA4j8xgUi29TpKXpm3whx5MW
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ETH 0xd433198cb786145767c67d874b36cd7d42baf57a
 
benzyme
#24 Posted : 1/27/2019 2:45:34 AM

analytical chemist

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found a troubleshoot for the issue.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
XMR 46JqfBqi7JNM1W5rXXZ1FF1CBKKLoGEVBRya9Cn3RJmPbQhT4GeZpVKWbwaVe4vUMveKAzAiA4j8xgUi29TpKXpm3whx5MW
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ETH 0xd433198cb786145767c67d874b36cd7d42baf57a
 
benzyme
#25 Posted : 2/14/2019 4:04:13 AM

analytical chemist

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did the jumper hack. system is back online, and operational.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
XMR 46JqfBqi7JNM1W5rXXZ1FF1CBKKLoGEVBRya9Cn3RJmPbQhT4GeZpVKWbwaVe4vUMveKAzAiA4j8xgUi29TpKXpm3whx5MW
BTC 3CNrz6Tj17U35GLkRB1zsNtVoedorw8oja
ETH 0xd433198cb786145767c67d874b36cd7d42baf57a
 
Loveall
#26 Posted : 2/14/2019 5:36:08 PM

šŸ’–

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Big grin Big grin Big grin Thumbs up Love
ā€œ... (a) psychedelic substance occasionally causes psychotic behaviour in people who have not taken it.ā€
Excerpt from a McKenna talk transcript / audio.
 
benzyme
#27 Posted : 7/19/2019 9:29:23 PM

analytical chemist

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fantastic news: after three years of owning this instrument, I finally found a way to correct for mass accuracy. No engineers, no Ph.Dā€™s, not even my own mentor could help me. I 100% figured it out in diagnostics...manually set the Main RF Frequency.
benzyme attached the following image(s):
DMT.JPG (178kb) downloaded 72 time(s).
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
XMR 46JqfBqi7JNM1W5rXXZ1FF1CBKKLoGEVBRya9Cn3RJmPbQhT4GeZpVKWbwaVe4vUMveKAzAiA4j8xgUi29TpKXpm3whx5MW
BTC 3CNrz6Tj17U35GLkRB1zsNtVoedorw8oja
ETH 0xd433198cb786145767c67d874b36cd7d42baf57a
 
Mindlusion
#28 Posted : 7/19/2019 9:31:03 PM

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benzyme wrote:
fantastic news: after three years of owning this instrument, I finally found a way to correct for mass accuracy. No engineers, no Ph.Dā€™s, not even my own mentor could help me. I 100% figured it out in diagnostics...manually set the Main RF Frequency.


Great news, glad to hear this Thumbs up
Expect nothing, Receive everything.
"Experiment and extrapolation is the only means the organic chemists (humans) currrently have - in contrast to "God" (and possibly R. B. Woodward). "
He alone sees truly who sees the Absolute the same in every creature...seeing the same Absolute everywhere, he does not harm himself or others. - The Bhagavad Gita
"The most beautiful thing we can experience, is the mysterious. The source of all true art and science."
 
benzyme
#29 Posted : 7/19/2019 9:32:55 PM

analytical chemist

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thanks Thumbs up

so what does this mean? I'll calibrate for standards, to give peace of mind results.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
XMR 46JqfBqi7JNM1W5rXXZ1FF1CBKKLoGEVBRya9Cn3RJmPbQhT4GeZpVKWbwaVe4vUMveKAzAiA4j8xgUi29TpKXpm3whx5MW
BTC 3CNrz6Tj17U35GLkRB1zsNtVoedorw8oja
ETH 0xd433198cb786145767c67d874b36cd7d42baf57a
 
tatt
#30 Posted : 7/20/2019 4:55:34 AM
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benzyme wrote:
fantastic news: after three years of owning this instrument, I finally found a way to correct for mass accuracy. No engineers, no Ph.Dā€™s, not even my own mentor could help me. I 100% figured it out in diagnostics...manually set the Main RF Frequency.


Thumbs up Cool
 
benzyme
#31 Posted : 2/12/2020 5:32:31 AM

analytical chemist

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I quit my job...
this means, I can devote more time to consultation. I just changed the electron multiplier, so the sensitivity is back to where it needs to be. I can/will process any samples coming my way, with quicker turnaround time.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
XMR 46JqfBqi7JNM1W5rXXZ1FF1CBKKLoGEVBRya9Cn3RJmPbQhT4GeZpVKWbwaVe4vUMveKAzAiA4j8xgUi29TpKXpm3whx5MW
BTC 3CNrz6Tj17U35GLkRB1zsNtVoedorw8oja
ETH 0xd433198cb786145767c67d874b36cd7d42baf57a
 
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