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just some xtals Options
 
Samvidbuho
#281 Posted : 4/1/2019 1:23:28 AM

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Separated the crystals from the last pic, the one with the white crystals has been suspended for 60 hrs without moving from suspension, but the other one has shaped up pretty well..
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STS is a community for people interested in growing, preserving and researching botanical species, particularly those with remarkable therapeutic and/or psychoactive properties.
 
Samvidbuho
#282 Posted : 4/3/2019 11:18:47 PM

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I'll add another, from a separate batch. Single re-x in hexane, doing FASA method, fairly sure the hexane was used to pull directly from the freebase|carbonate - water solution and transfered directly to crystallizing dish.
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Samvidbuho
#283 Posted : 5/13/2019 7:14:03 PM

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New Techniques
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endlessness
#284 Posted : 5/14/2019 10:46:26 PM

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Beautiful!

Thanks for sharing!
 
Orion
#285 Posted : 11/1/2019 8:05:06 PM

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This is a recent conversion from fumarates back to freebase, a semi a/b (?) with standard room temp naphtha pulls. Quite happy with the big cluster! Most of it formed at room temperature after some evaporation of the very clear naphtha.
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Art Van D'lay wrote:
Smoalk. It. And. See.
 
Metta-Morpheus
#286 Posted : 11/1/2019 9:37:16 PM

Fly with the sea birds and sh!t

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^❤️❤️🍆😉
“You think that’s air you’re breathing?” -Morpheus
“Whoa fellas, I’m feeling kinda bowling ball-ish.” -Leopold Butters Stoch
It’s got what plants crave. -Brawndo

Magic is here for us all to feel. Naming it isn’t what makes it real.
Running around for us all to know, noticing isn’t what makes it so... -Avett Brothers
 
Mindlusion
#287 Posted : 12/2/2019 5:13:43 PM

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.
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Expect nothing, Receive everything.
"Experiment and extrapolation is the only means the organic chemists (humans) currrently have - in contrast to "God" (and possibly R. B. Woodward). "
He alone sees truly who sees the Absolute the same in every creature...seeing the same Absolute everywhere, he does not harm himself or others. - The Bhagavad Gita
"The most beautiful thing we can experience, is the mysterious. The source of all true art and science."
 
Jagube
#288 Posted : 12/2/2019 5:34:46 PM

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You'll have to break that bottle to get them out Pleased
 
Metta-Morpheus
#289 Posted : 12/2/2019 7:20:00 PM

Fly with the sea birds and sh!t

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They look like quartz crystals 🤤

What substance is that?
“You think that’s air you’re breathing?” -Morpheus
“Whoa fellas, I’m feeling kinda bowling ball-ish.” -Leopold Butters Stoch
It’s got what plants crave. -Brawndo

Magic is here for us all to feel. Naming it isn’t what makes it real.
Running around for us all to know, noticing isn’t what makes it so... -Avett Brothers
 
Mindlusion
#290 Posted : 12/3/2019 5:54:23 AM

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Metta-Morpheus wrote:
They look like quartz crystals 🤤

What substance is that?


A certain substituted beta-nitrostyrene, I developed some new reaction conditions with the goal of improving yield and reducing the use of excess reagents, after warming slightly, leaving the reaction at room temperature over the weekend gave these results as a great success. Crystallization seeded on the stirbar. It does look like quartz. I've never seen a nitrostyrene crystal this big, hell, i've never seen crystals of any organic molecule this big. Dense and heavy as well, The crystals in the tray weighed 14.5g, the large one weighed 1.26g. 6cm length, 1cm wide, just under 0.5cm thick. Wow.
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Expect nothing, Receive everything.
"Experiment and extrapolation is the only means the organic chemists (humans) currrently have - in contrast to "God" (and possibly R. B. Woodward). "
He alone sees truly who sees the Absolute the same in every creature...seeing the same Absolute everywhere, he does not harm himself or others. - The Bhagavad Gita
"The most beautiful thing we can experience, is the mysterious. The source of all true art and science."
 
Metta-Morpheus
#291 Posted : 12/3/2019 12:08:18 PM

Fly with the sea birds and sh!t

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So you said that was kryptonite? Is your name Lex?
“You think that’s air you’re breathing?” -Morpheus
“Whoa fellas, I’m feeling kinda bowling ball-ish.” -Leopold Butters Stoch
It’s got what plants crave. -Brawndo

Magic is here for us all to feel. Naming it isn’t what makes it real.
Running around for us all to know, noticing isn’t what makes it so... -Avett Brothers
 
PurpScurp
#292 Posted : 6/10/2020 8:33:03 PM

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I just got promoted yay, and THIS is the thread i've been excited to participate in because I do photography, so here's pics of my recent snow globes. Nothing big, but my next step is to do some re-x and grow big ones.

I have a question about re-x (i'll be using naptha): for big crystals should I freeze precipitate or do a slow room temp evap? I've seen both suggested. I'm planning on the slow evap but let me know if you think freeze precip is better.
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coAsTal
#293 Posted : 6/10/2020 8:41:15 PM

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Gorgeous work PS--

Slow evap will always make the densest, largest crystals-- the colder it is the liklier it is to crash out in multiple places making each one smaller, but I've made 1/2" glass shards before with room-temp evap using heptane-- took about a month but they were HUGE.
 
PurpScurp
#294 Posted : 6/10/2020 9:37:43 PM

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coAsTal wrote:
Slow evap will always make the densest, largest crystals-- the colder it is the liklier it is to crash out in multiple places making each one smaller, but I've made 1/2" glass shards before with room-temp evap using heptane-- took about a month but they were HUGE.


Ouf, that sounds great, alright thanks for the advice.
 
tripwire
#295 Posted : 6/26/2020 12:48:46 PM
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spice fumarate re-x from boiling IPA Love

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null24
#296 Posted : 6/26/2020 4:10:13 PM

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PurpScurp, you have my vote to nominate you to be the official photographer for DMT.

Not the DMT nexus, DMT period.Thumbs up

Love this stuff, beautiful, inspiring, and educational!Love
Sine experientia nihil sufficienter sciri potest -Roger Bacon
*γνῶθι σεαυτόν*
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