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Psilocybin chromatography/solid phase extraction Options
 
Creachemist
#1 Posted : 8/17/2019 11:51:05 AM

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Joined: 17-Aug-2019
Last visit: 15-Jun-2020
Firstly i want to appologise for my grammar mistakes, i am dutch and never that good at languages because fysics and sience always got and gets my vote.

Secondly i want to thank everyone on this forum especially benzene i have scouerd for hours maybe days on this site and even rigged op my own vac destillation aparatus wrote little books about dmt, mescaline, bufotenine en psilocybin extractions en 99% of the information that is in there came from te nexus so thank you all very muchy.

This is my first post as a member and please note i am not a chemist its juist that extractions are mij hobby/guilty plessure

My question is, i want to purify psilocybin i am not started yet but is want te be well perpared is it possible to make a chromatography setup by loading a column with cotton balls and using (non-lab only) chemicals te release is, kind of like SPE (solid phase extraction) and te persieve the collers is it juist as simple as shining a uv light on it or is it more than that?

Thank you if you can help me with this one because is a little headache for a while now😄
 

STS is a community for people interested in growing, preserving and researching botanical species, particularly those with remarkable therapeutic and/or psychoactive properties.
 
Loveall
#2 Posted : 8/17/2019 2:13:35 PM

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Chemical expertSenior Member

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Creachemist wrote:
Thank you if you can help me with this one because is a little headache for a while now😄


Welcome to the club brother 😅

There is some ongoing work along these lines using cation resin. Never go alkaline, avoid light, elute with a volatile salt (ammonium acetate), and it looks like we will need to freeze and sublimate at the end. Using HPBCD to try to stabilize psilocin is also being looked at.

We've done a few pieces of his but need to put it together and see if it works. Have you seen the posts on this? Should be available by searching for cation resin. There are 2010/11 papers we are trying to emulate also. Tryptophan supplement powder may be a good way to test out resin binding/eluting conditions before burning through mushrooms with experiments.

One issue is that a lot of things in the mushrooms glow in UV, so eyes won't cut it I think. A reagent to test the column fractions may be better for us who don't have a spectrometer. Here is an example of ongoing work.

And welcome to the Nexus!
“... (a) psychedelic substance occasionally causes psychotic behaviour in people who have not taken it.”
Excerpt from a McKenna talk transcript / audio.
 
Creachemist
#3 Posted : 8/18/2019 12:59:41 AM

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Posts: 15
Joined: 17-Aug-2019
Last visit: 15-Jun-2020
Wow thanks man i feel home since my love for dmt dates from 3 years ago but now i finally have the knowledge (to my perspective) that i can add something to this forum i will check it out immidiatly thanks for your effort!
 
fathomlessness
#4 Posted : 8/20/2019 2:23:39 AM

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Posts: 956
Joined: 24-Jan-2015
Last visit: 09-Jan-2021
Loveall wrote:
Creachemist wrote:
Thank you if you can help me with this one because is a little headache for a while now😄


Welcome to the club brother 😅

There is some ongoing work along these lines using cation resin. Never go alkaline, avoid light, elute with a volatile salt (ammonium acetate), and it looks like we will need to freeze and sublimate at the end. Using HPBCD to try to stabilize psilocin is also being looked at.

We've done a few pieces of his but need to put it together and see if it works. Have you seen the posts on this? Should be available by searching for cation resin. There are 2010/11 papers we are trying to emulate also. Tryptophan supplement powder may be a good way to test out resin binding/eluting conditions before burning through mushrooms with experiments.

One issue is that a lot of things in the mushrooms glow in UV, so eyes won't cut it I think. A reagent to test the column fractions may be better for us who don't have a spectrometer. Here is an example of ongoing work.

And welcome to the Nexus!


Is it still that unstable when manufactured in lab conditions? Do they end up with a pure product/powder? (ie with the trials currently being done)
 
 
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