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Naphta layers didn't separate. What ti do now Options
 
Dimitri096
#1 Posted : 8/7/2019 9:34:14 AM
Hi i followed dmt handbook tek and when the layers should have separated they didn't
Can I try again without dumping the basified solution?
Do I have to re heat it up?
Please help me I don't want to throw everything awaySad
 
Northerner
#2 Posted : 8/7/2019 9:44:20 AM
Add more base. Commonly that's the issue with first extractions.
The nearest we ever come to knowing truth is when we are witness to paradox.
 
Achilles
#3 Posted : 8/7/2019 9:52:08 AM
Keep in hot water... I’d try adding more naphtha and keeping it warm this time and see if you can get a pull.. if not scrap it and start over
This guys ego ^
 
Northerner
#4 Posted : 8/7/2019 10:11:07 AM
Even after you've heated and added base, you can still add salt even which can sometimes help.

I wouldn't scrap a soup unless it had sat there for months and still not separated, which I am yet to see.
The nearest we ever come to knowing truth is when we are witness to paradox.
 
Dimitri096
#5 Posted : 8/7/2019 10:32:49 AM
Okay thanks and should I heat in in the tank or put it back in the saucepan??
 
Achilles
#6 Posted : 8/7/2019 10:38:24 AM
I just put my jar in a pot of hot tap water.. always works for me
This guys ego ^
 
Dimitri096
#7 Posted : 8/7/2019 1:47:02 PM
Is It normal that when I shake it it gets foamy?
I'm trying adding salt first and I put some of the tea in a glass jar inside a hit water pan
If it doesn't still work I'll try to falsify more
What do you suggest? And when I shake I have to let it sit for a minute in between but with open or closed cap?
Oh and the foam doesn't never go away afteri shacked
Thanks
 
endlessness
Moderator
#8 Posted : 8/7/2019 2:01:56 PM
Check the FAQ , so many of these questions are answered there.

Good luck
 
Mushroom Whisperer
#9 Posted : 8/7/2019 3:08:03 PM
Don't shake it! Stir with a large spoon. That's probably why you're having this problem.
 
Mushroom Whisperer
#10 Posted : 8/7/2019 3:09:32 PM
Actually I know it's the problem.
 
fulger
#11 Posted : 9/15/2019 4:38:49 AM
Northerner wrote:
Even after you've heated and added base, you can still add salt even which can sometimes help.

I wouldn't scrap a soup unless it had sat there for months and still not separated, which I am yet to see.



I have had 60ml naphtha not separate from a jar of 50g mhrb powdered and 50g lye with 300ml h2o. I left it sit for a week and still didn't separate and I tried heating in warm h2o and nothing. I added another 60ml naphtha and that would separate but I didn't get a good yield. I got 0.121 of dry white spice.
 
 
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