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Please help! Might have pulled a little base into pyrex Options
 
Juliusx33
#1 Posted : 6/4/2019 9:11:26 PM
Ok so I’m doing a STB extraction and am on my third pull. When I used my pipette to suck the Heptane off, I think I got a drop or two of my bass (it was light brown). It looks clear now but how should I proceed from here? I have been putting my pulls in a glass dish thus far. Should I just continue and then re-crystalize?
 
DreadedShaman
#2 Posted : 6/4/2019 9:27:39 PM
It seems to me that you have the right idea, I would just finish my extraction and then re x to clean up anything
 
Juliusx33
#3 Posted : 6/4/2019 9:33:36 PM
DreadedShaman wrote:
It seems to me that you have the right idea, I would just finish my extraction and then re x to clean up anything


Thank you! I was going to instead after all my pulls, pour it all in a shot glass with base and separate again. However, there seems to be crystals already forming.
 
Juliusx33
#4 Posted : 6/4/2019 9:45:31 PM
Here it is
 
Juliusx33
#5 Posted : 6/4/2019 9:53:11 PM
SORRY
Juliusx33 attached the following image(s):
IMG_2191.jpg (2,064kb) downloaded 56 time(s).
 
Juliusx33
#6 Posted : 6/5/2019 2:43:05 AM
Everything is okay, going for a re-crystallization!
 
BigJungleBuds
#7 Posted : 6/5/2019 3:23:09 AM
It looks like there is nothing there or a verry small amount of melted and not properly formed dmt solids that have melted?? so you should probably first try to yield a good enough amount of dmt if you are wanting to do a proper re x also if you have any naps in your dish you can always at the end before freeze pour your solvent from your dish you have base in into something else then wash the dish and dry and put it back or just use another dish Cool
 
Juliusx33
#8 Posted : 6/5/2019 3:52:16 AM
BigJungleBuds wrote:
It looks like there is nothing there or a verry small amount of melted and not properly formed dmt solids that have melted?? so you should probably first try to yield a good enough amount of dmt if you are wanting to do a proper re x also if you have any naps in your dish you can always at the end before freeze pour your solvent from your dish you have base in into something else then wash the dish and dry and put it back or just use another dish Cool


Yeah that picture was after one pull because it was my first time using the pipette and I couldn't figure the damn thing out Embarrased So crystals starting slowly forming because it starting evaporating quicker than I thought. Now have four pulls in the freezer and I checked recently, its looking gooooooood. After I freeze precipitate, going to Re x with some warm heptane Smile Cheers Thumbs up
 
 
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