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DM acetate: evaporation drying and transformation into free base. advise for finali (1x noob) Options
 
greg170985
#1 Posted : 3/20/2019 7:33:39 PM
Hello everyone and thank you in advance for your answer
I AM FRENCH SO I AM EXECUTING ME IN ADVANCE IF THE TRANSLATION IS BAD

after a first attempt at STB xylene extraction I have problems to crystallize and harvest my dmt.

so i post a question here on the forum: https: //www.dmt-nexus.me/forum/default.aspx? g = posts & m = 968788 & # post968788
Or it is advisable to make my xylene sweater with a mixture of water distill vinegar that worked well ...
may have evaporation I encountered some problem because I was told to "reduce to powder ..." (SEE THE DISCUSSION OF THE PREVIOUS TOPIC THIS WILL HELP YOU BETTER UNDERSTAND MY SITUATION) blow to drying the product appeared It may not be completely dry, but it may remain resinous even when it is still cold. It may still look like black resin that is less sticky than hot, but it may still be a little hot so it was "wet" not powdered or dry.
so I had it reduced to get a plate that I stink and break down to achieve the result adviser may give me the impression that it was burning ...
moreover I do not notice reaction with the mixture carbonate waters of more than once in the solvent that to keep its hard form all is not well diluted in the alcohol ....
can you tell me the reaction to wait with the mixture carbonate waters and the same concerning the dilution of years the alcohol that must it pass to you?

I was expecting to be able to powder after complete evaporation of the blow I think I have too much force on drying can you confirm me or not I beg you

can not wait to read you to finally finalize ... !!! this first extraction of my life and finally be able to enjoy the precious molecule
a big thank you to those who will answer I can not wait to finish drying this dmt acetate convert and finally enjoy:




bonjour a tous et merci d'avance pour vos réponse
JE SUIS FRANÇAIS DONC JE M'EXCUSE D'AVANCE SI LA TRADUCTION EST MAUVAISE

après une première tentative d’extraction STB au xylène j'ai rencontrer des problème pour cristalliser et récolter ma dmt.

j'ai donc poster une question ici sur le forum :https://www.dmt-nexus.me/forum/default.aspx?g=posts&m=968788&#post968788
ou l'on ma conseiller de faire des pull de mon xylène avec un mélange eau distiller vinaigre qui a bien marcher...
mai a l'évaporation j'ai rencontre quelque problème car l'on ma dit de "réduire en poudre..." (VOIR LA DISCUSSION DU TOPIC PRÉCÉDENT CELA VOUS AIDERA A MIEUX COMPRENDRE MA SITUATION ) du coup au séchage le produit est apparue mai na pas sécher complètement il rester résineux même une fois froid cela ressembler encore a de la résine noire moins collante que chaude mai encore un petit peut du coup était elle "humide" pas en poudre ou sèche ?
du coup je l'ai fait réduire jusque obtenir une plaque que j'ai pue briser et réduire en poudre afin d’atteindre le résultat conseiller mai cela ma donner l'impression que c’était brûler...
de plus je n'est pas remarquer de réaction avec le mélange carbonate eaux de plus une fois dans le solvant cela a garder sa forme dure tout ne c'est pas bien diluer dans l'alcool....
pouvez vous me dire la réaction a attendre avec le mélange carbonate eaux et pareil concernant la dilution d'ans l'alcool que doit t'il ce passer ?

je m'attendait a pouvoir réduire en poudre après évaporation complète du coup je pense avoir trop forcer sur le séchage pouvez vous me confirmer ou pas je vous prie

impatient de vous lire afin de finaliser enfin...!!! cette première extraction de ma vie et enfin pouvoir profiter de la précieuse molécule
un grand merci a ceux qui vont répondre j'ai très hâte de finir de faire sécher cette dmt acétate la convertir et enfin en profiter Very happy
peace
 
downwardsfromzero
ModeratorChemical expert
#2 Posted : 3/20/2019 8:34:54 PM
Mix the acetate resin with dry sodium carbonate powder, then add a drop or two of water to make a paste.
Stir well to ensure thorough reaction, then allow to dry again.
Wash with several minimally sized portions of alcohol.
Allow the alcohol to evaporate in a shallow dish.

Hopefully you'll be left with some kind of goo after this procedure.
An alternative might be to pull with warm naphtha instead of ethanol, then you can put it in a jar in the freezer.


Patience, patience, patience!

Bon chance!




“There is a way of manipulating matter and energy so as to produce what modern scientists call 'a field of force'. The field acts on the observer and puts him in a privileged position vis-à-vis the universe. From this position he has access to the realities which are ordinarily hidden from us by time and space, matter and energy. This is what we call the Great Work."
― Jacques Bergier, quoting Fulcanelli
 
greg170985
#3 Posted : 3/20/2019 8:54:28 PM
perfect thank you for the precision I understand better proceed as follows: grin:
do you talk about pulling my xylene with hot napht this is it?

in any case perfect I'm going away not finish this to be able to enjoy all this weekend: p
thank you again for all your advice it's nice to find help so quickly: d: d


 
greg170985
#4 Posted : 3/20/2019 8:56:53 PM
I would give news of my different extraction and product quality soon
 
downwardsfromzero
ModeratorChemical expert
#5 Posted : 3/20/2019 11:45:15 PM
Quote:
do you talk about pulling my xylene with hot napht this is it?

Context. And surely you realise xylene and naphtha are 100% miscible?

You're going to have to start doing your own homework, I'm afraid ("Je suis désolée").




“There is a way of manipulating matter and energy so as to produce what modern scientists call 'a field of force'. The field acts on the observer and puts him in a privileged position vis-à-vis the universe. From this position he has access to the realities which are ordinarily hidden from us by time and space, matter and energy. This is what we call the Great Work."
― Jacques Bergier, quoting Fulcanelli
 
 
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