Ok, as SWIM attempted to extract DMT using Cyb's Hybrid ATB Salt Tek yesterday, he experienced an emulsion with the heptane and decided to let the brew rest for a time to clear it up. Now it seems that crystals have fully formed in the solvent, in the bottle. Crystals white and pure as the driven snow. Only problem is, Swim has no idea how to get them out without getting the black goo mixed in with it. Any ideas? MNL attached the following image(s):  1.jpg (1,486kb) downloaded 62 time(s). 2.jpg (1,517kb) downloaded 61 time(s). 3.jpg (1,913kb) downloaded 61 time(s).
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I used lye and naphtha, and I kinda gave up on it after I started it, figured it was a lost cause cuz I did it, but a couple weeks later it started to grow crystals, very similar to yours, I just sucked up all the top layer with a nice syringe turkey baster kinda thing from a supermarket, metal tip, cut the tip flush and sucked out the top layer, my last stage was just freezing so I wanted the entire top layer in a dish anyway, the fact that there were crystals in it didn't really make a difference, but I had to carefully pick a couple out of the threshold between layers where they were enlodged, it took some dark crap with em but I put all the clear in a dish and tilted it back and forth rinsing the dark out some, but I'll tell ya, those crystals dark or not didn't matter, packed some really nice punch, your method isn't the same as mine but I hope my response was some help, good luck and be patient
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think since you have so many crystals on the border you might want to heat the solution to about 130 degrees f and shake it good and let it cool gradually and separate it before it has a chance to form crystals again, but I'm no expert, my best advice is to research this site, he's...one if a kind, he's covers all the bases https://vimeo.com/belovenet/videos
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