200 HBWR were finely ground, and allowed to soak in bestine over night. The bestine was filtered out and set aside,I just went to put moar bestine in and I accidentally added water instead....what can/should I do ...PLZ help is it - 7 hits or dosing 7 times ..... Either way I lost count along time ago, and Just type/Speak without a filter.... All of this is just one big tasty 'word salad'......
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Post the procedure you're following.
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It was suppose to be similiar to the PAnormix but I didnt follow an exact procedure. I never do with most of my extractions, I usually study many similiar and use different styles that I understand best.I do not have access to naptha so Bestine was used instead.200 HBWR ground were soaked for 20 hrsand then filtered through a sock. All of the seed mush was placed back in the vessel and I was planning on soaking the seeds 2 moar times over night in bestine as well. I was also planning on drying the seeds and soaking in acetone, followed by a filter X3 , and an evap. When the water was accidentally placed in the vessel today, most of the bestine was filtered out but there was a tiny amount left. I have heard LSA is water soluable so I went ahead and shook my vessel , filtered the water and repeated -until the water became very clear. I placed a little bit more water and I am going to let it sit overnight and do 2 more pulls tomorrow, or more until the water is crystal clear, its close as is. I am now left with about 10oz. of thick syrup-ish brown water with a 2cm layer of fat?/bestine on top. What can be done with this water? Should I remove the bestin, and can I just add Aceton or IPA straight too it and pull from that or am I going to have to evap it before I can play with it... .Any help would be greatly appreciated. is it - 7 hits or dosing 7 times ..... Either way I lost count along time ago, and Just type/Speak without a filter.... All of this is just one big tasty 'word salad'......
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I am just wondering that If the water did pull the alkaloids, Can I pull those alkaloids from that water using acetone or IPA or am I going to have to evaporate? is it - 7 hits or dosing 7 times ..... Either way I lost count along time ago, and Just type/Speak without a filter.... All of this is just one big tasty 'word salad'......
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How are you going to pull from the water with acetone or IPA? They're both miscible with water.
I guess you could wash your water solution with bestine as long as it's somewhat acidic. After that, you could evap or try basifying and extracting with NP.
I'm guessing here, based on what I've read, not personal experience.
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that's a good call, pretty much what I would do. as long as the water is somewhat acidic, the bestine shouldn't have any alkaloids. basify with ammonia, and pull with dcm or xylene. "Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
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