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layers not separating
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terrible_gibberish
#1
Posted :
2/27/2012 9:03:31 PM
Hi all. Im doing a STB using naphtha and hydroxide. Last night i used a separatory funnel to try and separate the layers. After so, about half of the naphtha came out afterwards. Now im trying to do a 2nd pull, but cant seem to get the layers to separate again.
Do i want to add more basified water or what? i know theres a basic rule. I estimate i added 2-3 liters of basified water+ 275 grams MHRB and about a liter or so of naphtha. Any ideas? I know theres a fix for it
۩
#2
Posted :
2/27/2012 9:10:31 PM
Yes you need to add more base.
terrible_gibberish
#3
Posted :
2/27/2012 9:17:46 PM
OK, so then my plan is to drain half my solution into another Milk jug then add maybe a liter or so of more basified water. crossing my fingers. dont wanna waste product u know
terrible_gibberish
#4
Posted :
2/27/2012 9:27:33 PM
heres what it looked like last night btw
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