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improvising teks..can mean loss :( Options
 
vapormeister
#1 Posted : 2/4/2012 3:01:12 AM
I went in with a friend who introduced me to DMT years ago.. maybe.. because that stuff hit harder and was yellow and hard chards..like nothing I can make.. posssible been bufotenin. Now I have to get on here because the idiot was on here and coulndt resist politics. My theory is ignorance is bliss, I will die when its my time. that said, after getting a sep funnel, and having some past experience in chemistry, did a A/B method with 300g. i did h20/gar 3/1 ratio in a crockpot. We did 3 boils then i was on own. I reduced the liquid after using a percolator to get all the sludge to where it was a semitransparent red. I have a couple 800ml beakers i was working with to go back and forth. being that the sep funnel was 500ml (dam i was cheap..should got the 1 ltr) I had read that the liquid should be hot wiht naptha. Instead of mixing NaOH with water ahead of time which i did before on a STB and did not experience much heat. WHAT A DIFFERENCE IT MAKES when the liquid is hot and acidic! Been too long away from chemistry classes, i was thinking i would be making the PH neutral then base. I added about 10g at a time to about 50 gs to my 450ml of reduced salts serum which had just started cooling down from simmering in the pot in the beaker. ALL i could smell was DMT! the glass was hot to the touch just below boiling and about a third of what i used in stb! i didnt smell the lye just dmt..though that was odd. my ph papers read 14 wiht that little bit of lye. My first pull got about 600 mg. I used limonede on next pulls and wiht IPA got maybe 1.6g.

The bark was good. I learned to use a bigger stainless bowl for the Q21limtek then transfer the product to a smaller glass bowl after getting it to moist topsoil consistency(more fitting than cobbler crust) and I got 2% yeild

So your better off working with more liquid and doing 2 loads then to have a concentrated reaction with your acid burn up your dmt Sad

Hope this helps those "smart guys" who figure out too late that short cuts make for long delays
 
benzyme
Moderator | Skills: Analytical equipment, Chemical master expertExtreme Chemical expert | Skills: Analytical equipment, Chemical master expertChemical expert | Skills: Analytical equipment, Chemical master expertSenior Member | Skills: Analytical equipment, Chemical master expert
#2 Posted : 2/4/2012 3:18:04 AM
I need to work on an advanced tek; I contend a complete extraction can be conducted in an hour.

i improvise, but i have the right tools.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
 
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