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Elliot
#1 Posted : 6/15/2010 10:18:17 PM



This is the first time I've done an evaporation rather then a freeze precipitation.

I used sunnyside naptha.

The clear area is the are I scraped.


The rest is a yellowish wave.
I don't know what to do?
Is it smokable?
Will it dry away?
All of my posts are fictional.
 
antrocles
Senior Member
#2 Posted : 6/15/2010 11:07:10 PM
that looks like a LOT of plant fats and oils with very little crystalline DMT. some might call it 'jungle spice', but it just looks to me like something you're definitely gonna want to recrystallize....at least once anyways....

keep us posted!

L&G!!
"Rise above the illusion of time and you will have tomorrow's
wisdom today."
 
Elliot
#3 Posted : 6/15/2010 11:15:35 PM
If it's smokable I don't mind so much.
But thank you i will keep you posted.
All of my posts are fictional.
 
endlessness
#4 Posted : 6/15/2010 11:17:04 PM
maybe your naphtha has small amounts of aromatics (like xylene or similar) which makes it pull a more red fraction, possibly plant fats and oils as antrocles said. If that is it, it could be ok to smoke but it could also be somewhat harsh smoke, its hard to tell from a picture.

Did you do an evap test on your naphtha to see if it evaps clean, btw?
 
gammagore
#5 Posted : 6/15/2010 11:17:10 PM
Is that first picture of the a toilet?Smile

What tek did you use, and did you do a test evap of the naptha? how hot was the naptha when you pulled? It does look like ALOT of fats and oils.

Check to see if the naptha is clean. I wouldnt smoke that, clean it first and see what comes of that. Do a re-x and a SC wash if needed.
 
Elliot
#6 Posted : 6/15/2010 11:52:27 PM
No, that was a major mistake on my part as i always freeze precipitate.

I was about to place the bowl on the dry ice and i thought "iv'e never evaporated"

I will do a test right now.
All of my posts are fictional.
 
Elliot
#7 Posted : 6/16/2010 12:01:12 AM
haha and yes

I have the best lighting in my bathroom.
All of my posts are fictional.
 
Elliot
#8 Posted : 6/16/2010 12:06:24 AM


Just another image.
I scraped up most of it.


It's my second pull on 100 g mhrb using normans tek.
I let it sit for about 3 days though.

I recall when seeing the naptha in the turkey baster it was VERY yellow.

It was a urine yellow and very blurry.
All of my posts are fictional.
 
antrocles
Senior Member
#9 Posted : 6/16/2010 12:20:00 AM
whenever i've pulled anything dark yellow or red, i always do a sodium carbonate wash on it (usually 2 SC washes and a plain water wash) and that should get you to the 'pale pale yellow' point anyways.

freeze precip is definitely the way to get cleaner crystals though. evapping is gonna leave you with any fats and oils that may be present...which usually isn't a big deal if your pulls are moderately clean. in this particular case i think an SC wash would have been a good idea.

i also agree with endlessness that your solvent seems to have pulled a pretty good deal of stuff. could be that your naphtha has aromatics or sometimes heating naphtha super hot before pulling can wind up getting a bit more flotsam than you want.

either way, what you have there is totally clean-up-able.

BRING ON THE HEPTANE!! Pleased

L&G!!
"Rise above the illusion of time and you will have tomorrow's
wisdom today."
 
Elliot
#10 Posted : 6/16/2010 12:30:58 AM
Thanks for all the help!

Will continue to keep you guys posted.
All of my posts are fictional.
 
Elliot
#11 Posted : 6/16/2010 12:42:41 AM
any recommended brands of heptane?
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hyperspacing
#12 Posted : 6/16/2010 3:23:44 AM
Go to an art supply store and buy Bestine. Its sold as a rubber cement thinner/remover
-Close your eyes, See the light, and feel the sunshine in the shade

~All views, ideas and opinions of this user are strictly fictional and in no way represent an act done in reality.
 
Elliot
#13 Posted : 6/16/2010 4:21:53 AM
That works as a better solvent?
All of my posts are fictional.
 
antrocles
Senior Member
#14 Posted : 6/16/2010 5:10:07 AM
bestine is the best. it is pure heptane....bestine is just the brand name....

any good art supply place will have it...like hyperspacing said, it's a rubber cement remover. awesome for rextal and making changa because it evaporates so quickly and so completely.

L&G!!
"Rise above the illusion of time and you will have tomorrow's
wisdom today."
 
Elliot
#15 Posted : 6/16/2010 5:22:29 AM
alright,
thanks much guys !
All of my posts are fictional.
 
hyperspacing
#16 Posted : 6/18/2010 3:56:16 AM
heptane is nice and clean. extractions are a little trickier cuz you have to manage temperature but i havnt had to do a re-x since i started using it as a main puller.
-Close your eyes, See the light, and feel the sunshine in the shade

~All views, ideas and opinions of this user are strictly fictional and in no way represent an act done in reality.
 
 
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