I just boiled down a dilute tea I drink daily. I did a very simple distillation setup with a tube leading up then turned to cool with icepacks. The was a 'reflux' for a while since the tubing would instantly form condensation and return to starter. I also had trouble getting high temp on the liquid since my beaker isn't flat bottom so only outer edge would get the full heat.
A while back I watched a video of a guy that makes ayauhasca in batches of 150kg caapi. He had a few experiments on ideal temperatures and different things like extraction to know amounts and such. He got a liter of prepared caapi tea at 12:1 'mel' level or honey level and mentioned you shouldn't reduce a properly prepared tea further.
He had a lab distillation glass setup and simply started reducing the liquid further collecting the distillate in 200ml volumes and collected 3 vessels. Each had increasing reaction to black light indicating more and more harmalas lost in the vapor. He also did a different distillation on psychotria and suggested making the teas separately since you could want to reduce the psychotria with fresh water a few times to reduce the acidity.
I'll try to find his videos again. He doesn't go very deep in his experiments but shared some interesting things that I've not seen elsewhere.
https://youtu.be/Q7kfUWs_A9c?si=m2AAAtXZi7cfut8M&t=488