This is a bit confusing... you don't say which tek you followed, and you say it was extracted with naphtha, then extracted with toluene?
In any case, the ammonia wash has been
advised against several times due to many reports of loss of yield. If you want to wash your spice in the end, a sodium carbonate wash is preferred. Please read the
FAQ before continuing the thread, you might find your answers there.
(acacian was faster)
"The Menu is Not The Meal." - Alan Watts