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advice on a failed ACBR tek!! Options
 
clyde_frog
#1 Posted : 1/25/2013 12:02:50 AM
Clyde had great success with zinc dust, if the bark was too old. After time dmt oxidizes into dmt-n-oxide, which is insoluble in naptha. When u add the zinc dust into the acid step (clyde has only read about it being used with acetic acid, he doesn't know about any other) and shake it for two hours, the zinc dust snatches the oxide molecule from the dmt-n-oxide turning it back to dmt.

Or you could use another solvent, like xylene, which the oxide form is soluble in, if old bark is the problem.
All posts by clyde frog and his affiliates are fictional meanderings of the imagination of a fictional 8 yr old boy from a certain adult fictional comedy cartoon.
 
*oneironaut*
#2 Posted : 1/25/2013 4:28:58 PM
clyde_frog wrote:
Clyde had great success with zinc dust, if the bark was too old. After time dmt oxidizes into dmt-n-oxide, which is insoluble in naptha. When u add the zinc dust into the acid step (clyde has only read about it being used with acetic acid, he doesn't know about any other) and shake it for two hours, the zinc dust snatches the oxide molecule from the dmt-n-oxide turning it back to dmt.

Or you could use another solvent, like xylene, which the oxide form is soluble in, if old bark is the problem.


Thanks for the suggestion, I don't think the bark was old, but I will tray moving up to xylene and see if that pulls something... Confused
You can't do anything about yesterday, but you can do everything with tomorrow.

Everything I write on this forum is pure gibberish and fanciful nonsense!
 
*oneironaut*
#3 Posted : 1/27/2013 5:09:35 PM
No other ideas folks? There's got to be something more to this equation?

You can't do anything about yesterday, but you can do everything with tomorrow.

Everything I write on this forum is pure gibberish and fanciful nonsense!
 
 
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