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freeze precip results so far Options
 
OnceKnownNowFlown
#1 Posted : 8/3/2012 2:09:40 PM
Hiya guys.

So I left it to precip till morning, about 8 hours and this is what I've got so far. Curious about the big white glob, guess it can all be dried and cut up?
I realised there was waaaay too much solv for the tray so have poured some into another container to keep the level low.

Can I evap after freeze precip? It's hot here at the moment and could take advantage of the weather Smile

Pics to be added asap.
OnceKnownNowFlown attached the following image(s):
IMAG0187.jpg (1,115kb) downloaded 103 time(s).
 
cyb
Moderator | Skills: Digi-Art, DTP, Optical tester, Mechanic, CarpenterSenior Member | Skills: Digi-Art, DTP, Optical tester, Mechanic, Carpenter
#2 Posted : 8/3/2012 2:17:04 PM
Hey OKNF

The blob could be a water drop that has frozen...you will see if it melts later.
You really need 18-24hrs to be sure all the spice has precipt'd out...
I would just re-use the Nap for another pull or store for later...It shouldn't hold any more spice and would be a waste to evap to air..Very happy

If you mean can you evap the crystals after the nap is poured off...then I would recommend using a fan to quickly dry them....they will dissolve back into any remaining nap at warm temps..quicker the better..
Please do not PM tek related questions
Reserve the right to change your mind at any given moment.
 
Infundibulum
ModeratorChemical expert
#3 Posted : 8/3/2012 2:19:02 PM
What are we supposed to see here?



Need to calculate between salts and freebases? Click here!
Need to calculate freebase or salt percentage at a given pH? Click here!

 
OnceKnownNowFlown
#4 Posted : 8/3/2012 3:12:57 PM
Hopefully you can see the picture? Just making sure everythings looks alright so far.

Hey Cyb! Anything I can do about the globule? I am gonna be leaving it all in the freezer till about nine or ten tonight (24 hours then) and see what's what. I did manage to have a look at the naptha side on, looked very saturated/milky, so hoping for the best Smile
 
cyb
Moderator | Skills: Digi-Art, DTP, Optical tester, Mechanic, CarpenterSenior Member | Skills: Digi-Art, DTP, Optical tester, Mechanic, Carpenter
#5 Posted : 8/3/2012 3:17:58 PM
OnceKnownNowFlown wrote:


Hey Cyb! Anything I can do about the globule? I am gonna be leaving it all in the freezer till about nine or ten tonight (24 hours then) and see what's what. I did manage to have a look at the naptha side on, looked very saturated/milky, so hoping for the best Smile


Just leave it all as it is...see whats what later..if it is ice its no problem.
Please do not PM tek related questions
Reserve the right to change your mind at any given moment.
 
OnceKnownNowFlown
#6 Posted : 8/3/2012 3:31:03 PM
Thanks, will leave it be till tonight - if it is ice, do I melt and re-napth/precip on a smaller scale?
 
Psyren
#7 Posted : 8/3/2012 5:46:00 PM
remove the plastic wrap and take a closer pic.

and i think 24hrs is over kill if your solvent is saturated

how much bark and solvent did you use?
Seek not abroad, turn back into thyself, for in the inner man dwells the truth.
 
OnceKnownNowFlown
#8 Posted : 8/3/2012 6:46:13 PM
50g MHRB and about 45ml in each pull, total of 3 pulls - I will take another picture now Smile

Edit: I realised there was too thick amount of solvent (or so I thought) and decided to move some to another container, so hopefully I will yeild more that what is just in the baking try above, later on/tomorrow Smile


Seems to be a slightly sticky looking residue in there too. Guess its still the naptha?!
OnceKnownNowFlown attached the following image(s):
IMAG0188.jpg (1,232kb) downloaded 62 time(s).
 
OnceKnownNowFlown
#9 Posted : 8/3/2012 9:44:11 PM
I have a bad feeling about doing DMT right now. For some reason, when I came to vaping, I just had a moment of like, de ja vu. I don't know.
 
cyb
Moderator | Skills: Digi-Art, DTP, Optical tester, Mechanic, CarpenterSenior Member | Skills: Digi-Art, DTP, Optical tester, Mechanic, Carpenter
#10 Posted : 8/3/2012 9:47:41 PM
OnceKnownNowFlown wrote:

Seems to be a slightly sticky looking residue in there too. Guess its still the naptha?!


You will get some sticky in there as well..cant be helped though...just dry,dry,dry with a fan. It will all mix up when you scrape.
Nice white xtals though Very happy
Please do not PM tek related questions
Reserve the right to change your mind at any given moment.
 
OnceKnownNowFlown
#11 Posted : 8/3/2012 9:54:09 PM
cyb wrote:
OnceKnownNowFlown wrote:

Seems to be a slightly sticky looking residue in there too. Guess its still the naptha?!


You will get some sticky in there as well..cant be helped though...just dry,dry,dry with a fan. It will all mix up when you scrape.
Nice white xtals though Very happy


hey, yeah they came out great. my scales aren't brilliant, but it weighs 200mg... thats not even a starter on what i have in the freezer at the moment, expect about a gram or just over Smile hopefully i will feel okay tomorrow to take the step up... (that white glob was ice!)
 
 
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