So I'm doing my first re x on about a gram of yellow spice. Did the hot water bath with 20ml of naptha, dissolved the spice in the naptha.

Now the mixture is a nasty yellow, some gunk went to the bottom but it is still very yellow. Should I wait till it separates? or just decant it now into another shot glass?

decant now, freeze, repeat if necessary

already seeing crystals

Well there was lots of pretty white spice, poured out the naphtha, put it back in the freezer upside down for a few hours, took it out, put in under a fan, about 30 min later it started to melt so I stuck it back in the freezer.

Most likely do to the fact it was about 85 degrees in the house and all the naphtha wasn't gone yet. Will have to try again when I get off work.