so there is was.. using new limonene on a a/b solution that has biin sitting around for 3 weeks afte rthinking i boiled out the dmt adding naoh direct to to the hot acid water. i had to split the 300g MH extaction into 2 thick 350 ml bathces to use my 500ml sep funnel. after using the limo on both by emtpying the one bathc and adding the second. i eptied the last batch leaving a trace of lyewater which tis was so thick, could not get all from walls of sep funnel. I decided to wash lomi wiht socium carb water. After all its supposed to separate layers quickly and then you dump the water quickly to aviod DMT fallout...at least wiht NAPTHA.... I should of read this closer. I thought i could do a cleaning step before making my fumerate. I used water about 95F but was a llitle excessive wiht the soda, not measuring, so i added water to some i poured off into a different glass..it still felt "soapy"

THE BIG SUPRISE: I added about 100 mls of s carb water and shekd but the layer DID NOT seperate! if had a big viscoticy layer that looked like a nebula then parts of this cloud were dropping..like DAMN this is only 20 seconds now then i notice that crystals are dropping to the vavle of sepfunnel..i was thinking junk because itwas old solution, but i had np problem wiht layer separation before. I decided i better dump the water quick but put a glass under to save the water and catch those pieces of whatever. THEY WOULD NOT PASS THOURGH VALVE! somedi which i collected. the rest i had to get fater saving the limo and washed out wiht water. these are SHARDS...BIG ASS CHARDS like 2mm and better..shit that you wouldnt want the cops to see because they would think it to be the worse drug in USA.

SO i was able to collect most of what i had on a paper towel. i looked at the orage chards.WAY cleaner and bif then the crap i got from jimjam fumrate in s carb solution. So why did this happen? I am guessing my limo was SO saturated with DMT the DMT atached to the carb molecule and dropped.

The only problem wiht ths is getting the limo off so it does not remelt the dmt by touch. If i could figure a way to siphon off the limo off water and do in a beaker to where i could shake it,stir it or whatever and collect the flakes, this would be a way better way of getting freebase crystals from limo in my opinion.its easy succking off a bottom layer,but top layers are hard to do..like getting the fats off a stew. i could maybe break end off one of my pipetes so the chards would fit. but i am telling you,these are beutiful. I melted on pipe to check..defineily DMT

SO if you are looking to get chards out of limo i would suggest trying this. warm/hot carb water drect on our limo and watch the beauties fall

UPDATE:
I tried it on a 3rd pull q21 limtek and nothing happened. seems to be only on limo that is heavily saturated