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Big Xtals without evap? Options
 
PrimateSphinx
#1 Posted : 9/20/2011 7:03:29 AM
Hello all,

Swim has been extracting with noman's tek but has been using heptane instead of naptha for the entire process and precipitating in the fridge to get some pretty good-looking medium size pure crystals on the first go(no recrystalization needed). Swim wonders though if there is a way to get bigger crystals without evaporating the heptane to conserve it but still using something along the line of freeze precipitation.

Thoughts?
What are we but stupefied dancers to a discordant stystem, we believe - so we're mislead
we assume - so we're played
we confide - so we're deceived
we trust - so we're betrayed


 
endlessness
#2 Posted : 9/20/2011 8:31:41 AM
Yes, every hour or two, alternate the container between fridge and freezer, and between fridge and room temperature. When the temperature goes up, the smaller crystals dissolve first, and when you put it to a colder place, the new crystals tend to form on top of the bigger crystals that are already form, so you get nicer crystal formations. The more times you do this, the nicer crystals you will get
 
PrimateSphinx
#3 Posted : 9/20/2011 8:37:55 AM
Gracias Endlessness,

I will give it a try the next time some spice decides to extract itselfWink
What are we but stupefied dancers to a discordant stystem, we believe - so we're mislead
we assume - so we're played
we confide - so we're deceived
we trust - so we're betrayed


 
 
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