N6 wrote: I thought DMT is very soluble in it, certainly more so than in petroleum ether or xylene?
no.
maybe more soluble than pet. ether, but certainly not xylene. dmt is very soluble in xylene. this is the reason xylene is not effective in freeze precipitation, but naphtha is (I'd assume limonene as well)
and as long as you're not heating up the glass directly on a burner, you probably don't have to worry about breakage. limonene will not degrade glass, just heat up some water in the microwave, and let the container with limonene sit in it for a few minutes.
keep in mind, this is just to help you pull dmt from the basic water. you don't necessarily
need to heat the fumaric acid, it will readily complex with the free base alkaloids in the solvent, forming alkaloid salts.
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