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captdan
#1 Posted : 10/17/2023 7:28:10 PM
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Hi I have just dug out on old batch and itโ€™s turned into a red solid?
I did swap the container to a little plastic one. Did smoke a little but Iโ€™m feeling itโ€™s a little off or me paranoid lol.
 

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captdan
#2 Posted : 10/17/2023 7:31:26 PM
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Iโ€™m thinking if it reacted with the plastic container being the finished product how pure was it?
 
Homo Trypens
#3 Posted : 10/17/2023 7:54:17 PM

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If it did react with the plastic, i'd guess the most likely reason would be residual solvent.

It might have just oxidised or polymerised over time though.

Or something else i'm oblivious to and one of the more chemistry savvy nexians will mention soon Smile
 
navegandouniversos
#4 Posted : 10/20/2023 10:47:30 PM

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I once had a similar situation with a small amount of crystal, from what I read here in the Nexus, it had oxidized, (dmt n-oxide), or that I think about... here in the nexus you can read how to recover your free base, using zinc powder!
https://wiki.dmt-nexus.m...N-Oxide_to_Freebase_DMT
hugs !!!
 
downwardsfromzero
#5 Posted : 10/20/2023 11:52:48 PM

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Plasticizer could leach out of the plastic and accelerate oxidation/polymerisation, I suppose.

navegandouniversos makes a great suggestion with the zinc treatment; a mini A/B would be a good way of cleaning up plasticizer-contaminated material anyhow, so if it's a significant stash that you have this process should prove worthwhile.




โ€œThere is a way of manipulating matter and energy so as to produce what modern scientists call 'a field of force'. The field acts on the observer and puts him in a privileged position vis-à-vis the universe. From this position he has access to the realities which are ordinarily hidden from us by time and space, matter and energy. This is what we call the Great Work."
โ€• Jacques Bergier, quoting Fulcanelli
 
 
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