NullEntity wrote:From what i know most Recrystallization tek's dissolve spice in N-heptane via hot water bath and decanting leaving heavy impurities at the bottom...
NullEntity wrote:...i want a godly pure end result and loss of yield is the price to pay i understand that but the thought of the possibility making the process better keeps me up at night. There is a beautiful amount of extraction teks, but the methods for purifying are lacking in comparison, in my opinion. does any one know more on this ?
Hi NullEntity,
The whites are not really better than the yellows or the oils, really. All is dmt just another jacket. Get rid of the caustic, water wash if you feel so, very good, from then on you get very high quality deems.
Allow me to re-quote myself from an earlier post:
Quote:...Hopefully you're aware the goo is not to throw away, some people think it's impurities to discard, there is a hoax out there, it's very much very active dmt in oily form. If you're sure all caustic was out, it's blazingly usable...
Fancy white is cool candy looking, and there are some threads here to re-form oil to white texture, there is some progress but not really a golden bullet ideal workflow that nails it 100% each time, it's ongoing.
I bet water washing a spice loaded naphtha pull, or water washing a spice loaded re-x heptane, makes no difference. Only, Re-x is such a small volume that water washing that might affect separation of layers, but I havent tried that. If you're keen on water washing, why not the naphtha pull? You would grab any residual caustic there, and omit fuzzing with the small volume re-x heptane.
Happy trials...