downwardsfromzero wrote:I don't think chloroform is a very good suggestion for an alternative as it has direct and long term health hazards of its own.
If you're particularly worried about naphtha inclusions, redissolve your crystals in ethanol and leave to evaporate.
We`ve done conversion teks from fumarate to freebase using chloroform to grab nonpolars, it evaps extremely well. After heat dry and cut and re-heat-dry again it has no chloroform taste whatsoever (chloroform has a very recognizable sweet menthol taste). Tried the same with xylene and the taste diminishes after thorough drying, but it is in there.
downwardsfromzero`s great suggestion of redissolving in ethanol and evaporating will mostly switch some NPS out but leave some etoh in it, which is far more acceptable. And there`s no loss.
Same thing goes for fumarates, but you can do boiling IPA crystallization as a cleanup, or dissolve in water then evap.