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mass spec update Options
 
Loveall
#21 Posted : 12/27/2018 3:49:06 AM

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Thanks for trying benzyme. Smile
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benzyme
#22 Posted : 12/30/2018 3:30:24 AM

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I had a connector off by one pin Confused
it's operational now. I need a couple weeks before accepting samples. going to calibrate this week, and am on vacation next week.
-28 V fluctuates, but the instrument still functions. I'll work with it.
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"Nothing is true, everything is permitted." ~ hassan i sabbah
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Mindlusion
#23 Posted : 12/30/2018 7:07:18 PM

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benzyme wrote:
I had a connector off by one pin Confused
it's operational now. I need a couple weeks before accepting samples. going to calibrate this week, and am on vacation next week.
-28 V fluctuates, but the instrument still functions. I'll work with it.


damn!
Well all in all good news, hope to hear another good update
Expect nothing, Receive everything.
"Experiment and extrapolation is the only means the organic chemists (humans) currrently have - in contrast to "God" (and possibly R. B. Woodward). "
He alone sees truly who sees the Absolute the same in every creature...seeing the same Absolute everywhere, he does not harm himself or others. - The Bhagavad Gita
"The most beautiful thing we can experience, is the mysterious. The source of all true art and science."
 
benzyme
#24 Posted : 12/30/2018 7:18:52 PM

analytical chemist

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yeah. I started having issues after I did annual maintenance, broke the quartz spacer rings.
then I had problems getting adequate vacuum to turn on the ion optics, so I swapped out the helium line, because the brass connector was galled. I fixed the vac leak yesterday, then re-inspected the PS, that’s when I noticed the connector issue.

once I get comm initialized (hopefully this evening), I’ll calibrate. I gotta run a certain melatonin [fungal] product this week, hopefully I’ll have results by NYD.

The multipole offset voltages passed tests, something that’s never happened since I bought the instrument.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
benzyme
#25 Posted : 12/31/2018 3:58:12 AM

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Nexus
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"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
benzyme
#26 Posted : 1/2/2019 1:29:29 AM

analytical chemist

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Compare with fig. 2B
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"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
soul-explorer
#27 Posted : 1/2/2019 11:55:18 AM

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Very Nice Smile
 
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